The invention of radical reactions. Part XXXVI. Synthetic studies related to 3-deoxy-D-manno-2-octulosonic acid (KDO)

DOI: 10.1016/0040-4020(95)01089-0

Source and publish data:

Tetrahedron p. 2717 - 2726 (1996)

Update date:2022-08-30

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Authors:

Barton Barton

Jaszberenyi

Liu Liu

Shinada Shinada

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Article abstract of DOI:10.1016/0040-4020(95)01089-0

An application of the Barton ester based radical reactions in carbohydrate chemistry is described. The chain-elongation reaction with ethyl α-trifluoroacetoxy acrylate 2, followed by treatment with phenylhydrazine provided 3-deoxy-α-hydrazono-octulosonates 8a,b derivatives of KDO and its gluco-isomer in good yield.

Full text of DOI:10.1016/0040-4020(95)01089-0

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