Norbornadiene-Fused Heterocycles: Synthesis of 5,8-Dihydro-5,8-methanophthalazines and Regioselective Ring Cleavage and Skeletal Rearrangement of 6,7-Epoxy-5,6,7,8-tetrahydro-5,8-methanophthalazine 2-Oxides in Trifluoroacetic Acid

DOI: 10.1246/bcsj.71.497

Source and publish data:

Bulletin of the Chemical Society of Japan p. 497 - 502 (1998)

Update date:2022-08-31

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Authors:

Kobayashi, Tomoshige

Sugawara, Hideki

Nikaeen, Behrooz

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Article abstract of DOI:10.1246/bcsj.71.497

5,8-Dihydro-5,8-methanophthalazine, prepared by the reaction of bicyclo[2.2.1]hepta-2,5-diene-2,3-dicarbaldehyde with hydrazine, reacted with MCPBA to give an N-oxide. Further oxidation with MCPBA afforded the corresponding exo-6,7-epoxy derivative. Treat

Full text of DOI:10.1246/bcsj.71.497

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