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Methanesulfonic acid,hydrazide

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Name

Methanesulfonic acid,hydrazide

EINECS -0
CAS No. 10393-86-9 Density 1.401 g/cm3
PSA 80.57000 LogP 0.58130
Solubility N/A Melting Point 46-48 °C
Formula CH6N2O2S Boiling Point 229 °C at 760 mmHg
Molecular Weight 110.137 Flash Point 92.3 °C
Transport Information N/A Appearance N/A
Safety 15-26-36 Risk Codes 36/37/38
Molecular Structure Molecular Structure of 10393-86-9 (METHANESULFONYL HYDRAZIDE) Hazard Symbols R36/37/38:Irritating to eyes, respiratory system and skin.;
Synonyms

Mesyl hydrazide;

Article Data 16

Methanesulfonic acid,hydrazide Synthetic route

124-63-0

methanesulfonyl chloride

10393-86-9

methanesulphonyl hydrazide

Conditions
ConditionsYield
With sodium hydroxide; hydrazine hydrate In water at 8℃;90%
With hydrazine hydrate In tetrahydrofuran at 10 - 15℃; for 0.5h;82%
With hydrazine hydrate In ethanol at 10 - 20℃; for 1h;50%
124-63-0

methanesulfonyl chloride

A

10393-86-9

methanesulphonyl hydrazide

B

18300-37-3

di-methanesulfonyl hydrazide

Conditions
ConditionsYield
With sodium hydroxide; hydrazine hydrate In water cooling;
1201-93-0

1-phenyl-3-dimethylaminoprop-2-enone

10393-86-9

methanesulphonyl hydrazide

3708-04-1

2-methylsulfonyl-1-phenylethanone

Conditions
ConditionsYield
Stage #1: 1-phenyl-3-dimethylaminoprop-2-enone; methanesulphonyl hydrazide With tert.-butylhydroperoxide In water at 80℃; for 8h;
Stage #2: With copper diacetate In water
96%
2913-97-5

N-phthalimidyl-2-aminoacetaldehyde

10393-86-9

methanesulphonyl hydrazide

C11H11N3O4S

Conditions
ConditionsYield
In ethanol at 70℃; for 0.5h; Condensation;95%
10393-86-9

methanesulphonyl hydrazide

15436-11-0

(E)-methyl styryl sulfone

Conditions
ConditionsYield
With tert.-butylhydroperoxide; iodine; sodium carbonate In toluene at 90℃; for 3h; Inert atmosphere; stereoselective reaction;95%
With oxygen; copper(l) chloride; lithium bromide In dimethyl sulfoxide at 100℃; under 760.051 Torr; for 12h; Schlenk technique; stereoselective reaction;88%
120-72-9

indole

10393-86-9

methanesulphonyl hydrazide

2-(methylsulfonyl)-1H-indole

Conditions
ConditionsYield
With tert.-butylhydroperoxide; iodine In water; 1,2-dichloro-ethane at 20℃; for 2h; Green chemistry;92%
10393-86-9

methanesulphonyl hydrazide

51673-84-8

dimethoxyacetaldehyde

A

917918-89-9

(E)-N'-(2,2-dimethoxyethylidene)methanesulfonohydrazide

B

C4H10N4O4S2

Conditions
ConditionsYield
In tetrahydrofuran at 20℃; for 3.5h;A 91.1%
B n/a
119-61-9

benzophenone

10393-86-9

methanesulphonyl hydrazide

1244620-37-8

N'-(diphenylmethylene)methanesulfonohydrazide

Conditions
ConditionsYield
With hydrogenchloride In methanol; water for 24h; Reflux;90%
With hydrogenchloride In methanol; water for 1h; Reflux;
10393-86-9

methanesulphonyl hydrazide

(S)-2-amino-4-phenylbut-3-ene

C11H14O2S

Conditions
ConditionsYield
With palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In 1,4-dioxane at 20℃; for 24h;90%
10393-86-9

methanesulphonyl hydrazide

193536-85-5

(3R,3aS,4R,SR,7S,9R,9aR,12R)-3-methoxy-4,7,9,12-tetramethyl-8-oxo-7-vinyldecahydro-4,9a-propanocyclopenta[8]annulen-5-yl carbonochloridate

193536-97-9

(3R)-3-deoxo-11-deoxy-3-methoxy-11-oxo-4-epi-mutilin 14-[N-(methanesulphonylamino) carbamate]

Conditions
ConditionsYield
In dichloromethane89%

Methanesulfonic acid,hydrazide Specification

The Methanesulfonic acid,hydrazide, with the CAS registry number of 10393-86-9, is also known as Mesyl hydrazide. Its molecular formula is CH6N2O2S and molecular weight is 110.14. What's more, its IUPAC name is Methanesulfonohydrazide. In addition, it must be stored in airtight containers and placed in a dry, cool place.

Physical properties about the Methanesulfonic acid,hydrazide are: (1)ACD/LogP: -1.47; (2)# of Rule of 5 Violations: 0; (3)#H bond acceptors: 4; (4)#H bond donors: 3; (5)#Freely Rotating Bonds: 1; (6)Polar Surface Area: 49 Å2; (7)Index of Refraction: 1.491; (8)Molar Refractivity: 22.76 cm3; (9)Molar Volume: 78.5 cm3; (10)Surface Tension: 53.1 dyne/cm; (11)Density: 1.401 g/cm3; (12)Flash Point: 92.3 °C; (13)Enthalpy of Vaporization: 46.56 kJ/mol; (14)Boiling Point: 229 °C at 760 mmHg; (15)Vapour Pressure: 0.0711 mmHg at 25 °C.

Preparation: this chemical can be obtained by Methanesulfonyl chloride. The reaction needs reagent Hydrazine hydrate and solvent H2O. The reaction temperature is 8 °C. The yield is about 90 %.

The Methanesulfonic acid,hydrazide can be obtained by Methanesulfonyl chloride

Uses: it is used to produce other chemicals. For example, it is used to produce Phenyl methaneselenesulfonate. This reaction needs solvent CH2Cl2. The reaction time is 30 min. The yield is about 65 %.

The Methanesulfonic acid,hydrazide can react with Benzeneseleninic acid to get Phenyl methaneselenesulfonate

When you are using this chemical, please be cautious about it as the following:
As a chemical, it is irritating to eyes, respiratory system and skin. If contact with eyes accidently, rinse immediately with plenty of water and seek medical advice. In addition, during using it, wear suitable protective clothing.

You can still convert the following datas into molecular structure:
(1) SMILES: O=S(=O)(NN)C
(2) InChI: InChI=1/CH6N2O2S/c1-6(4,5)3-2/h3H,2H2,1H3
(3) InChIKey: VKHZYWVEBNIRLX-UHFFFAOYAS

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