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N-Methylcyclohexylamine
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Name

N-Methylcyclohexylamine

 EINECS 202-869-3
CAS No. 100-60-7 Density 0.868 g/cm3
PSA 12.03000 LogP 1.92940
Solubility 5.4 g/100 mL (20 °C) in water Melting Point -9--7 °C(lit.)
Formula C7H15N Boiling Point 146.5 °C at 760 mmHg
Molecular Weight 113.203 Flash Point 29.4 °C
Transport Information UN 2734 8/PG 2 Appearance clear colourless to yellow liquid
Safety 16-26-36/37/39-45 Risk Codes 10-21/22-35-20/21/22
Molecular Structure Molecular Structure of 100-60-7 (N-Methylcyclohexylamine) Hazard Symbols CorrosiveC
Synonyms

Cyclohexylamine,N-methyl- (6CI,7CI,8CI);(Methylamino)cyclohexane;Cyclohexylmethylamine;Methylcyclohexylamine;N-Cyclohexyl-N-methylamine;N-Cyclohexylmethylamine;N-Methyl-N-cyclohexylamine;N-Methylcyclohexanamine;NSC 434;

Article Data 99

N-Methylcyclohexylamine Synthetic route

108-94-1

cyclohexanone

124-40-3

dimethyl amine

A

100-60-7

N-methylcyclohexylamine

B

98-94-2

N,N-dimethyl-cyclohexanamine

C

108-93-0

cyclohexanol

Conditions
ConditionsYield
With hydrogen at 160 - 220℃; under 67506.8 - 97509.8 Torr; for 100 - 1000h; Product distribution / selectivity;A 0.1%
B 96%
C 0.5%
With hydrogen at 160 - 180℃; under 63756.4 - 97509.8 Torr; for 100 - 400h; Product distribution / selectivity;A 0.1%
B 94%
C 2%
109-73-9

N-butylamine

3-methyl-2-(N-methylcyclohexylamino)benzothiazolium iodide

A

70038-63-0

butyl-(3-methyl-3H-benzothiazol-2-ylidene)-amine

B

100-60-7

N-methylcyclohexylamine

Conditions
ConditionsYield
at 25℃; for 3h;A 95%
B 83%
In dichloromethane at 25℃; for 3h;A 95%
B 83%
931-53-3

Cyclohexyl isocyanide

100-60-7

N-methylcyclohexylamine

Conditions
ConditionsYield
With Zr12(μ3-O)5[(μ3-O)CoCl]8[(μ2-O)2(μ3-O)CoCl]3Li3(triphenyldicarboxylate)9; hydrogen In toluene at 110℃; under 30003 Torr; for 42h; Catalytic behavior; Inert atmosphere; Schlenk technique;92%
With dimethyl sulfoxide In water at 100℃; Green chemistry;65%
100-61-8

N-methylaniline

100-60-7

N-methylcyclohexylamine

Conditions
ConditionsYield
With hydrogen In neat (no solvent) at 80℃; under 7600.51 Torr; for 24h; Catalytic behavior; Autoclave;91%
With dichloro(μ-chloro)(μ-hydrido)bis(η-p-cymene)diruthenium(II); hydrogen In neat (no solvent) at 75℃; under 37503.8 Torr; for 24h;80%
With lithium; methylamine
593-51-1

methylamine hydrochloride

108-94-1

cyclohexanone

100-60-7

N-methylcyclohexylamine

Conditions
ConditionsYield
With iridium bromide; zinc In 1,4-dioxane; water at 30℃; for 72h;85%
With titanium(IV) isopropylate; sodium tetrahydroborate; triethylamine 1.) EtOH, 25 deg C, 10 h, 2.) EtOH, 25 deg C, 8 h; Yield given. Multistep reaction;
108-94-1

cyclohexanone

74-89-5

methylamine

100-60-7

N-methylcyclohexylamine

Conditions
ConditionsYield
With hydrogenchloride; Zr(BH4)2Cl2(dabco)2 In methanol for 1h; Heating;78%
With D-glucose; glucose dehydrogenase CDX-901; imine reductase 48 from Rhizobium sullae; nicotinamide adenine dinucleotide phosphate In aq. buffer at 25℃; for 24h; pH=9; Enzymatic reaction;66%
With sodium tetrahydroborate; lithium chloride In tetrahydrofuran; methanol Flow reactor; chemoselective reaction;37%
67-56-1

methanol

108-91-8

cyclohexylamine

100-60-7

N-methylcyclohexylamine

Conditions
ConditionsYield
With rhodium(III) chloride hydrate; potassium tert-butylate at 130℃; for 48h; Sealed tube; High pressure;75%
With thorium dioxide at 320℃;
rhodium hydrido (PEt3)3 complex for 10h;99 % Chromat.
With platinum on carbon; hydrogen; sodium hydroxide at 130℃; under 30003 Torr; for 36h; Autoclave;74 %Chromat.
With palladium 10% on activated carbon; potassium tert-butylate at 130℃; for 12h;
141339-38-0

N-(6-Methoxy-1,2,3,4-tetrahydro-naphthalen-1-yl)-N-methyl-hydroxylamine

100-60-7

N-methylcyclohexylamine

Conditions
ConditionsYield
With carbon disulfide In acetonitrile for 1.5h; Ambient temperature;71%
15267-95-5

chloromethyltriethoxysilane

108-91-8

cyclohexylamine

100-60-7

N-methylcyclohexylamine

Conditions
ConditionsYield
Stage #1: chloromethyltriethoxysilane; cyclohexylamine at 87℃; for 18h;
Stage #2: With water In ethanol for 48h; Heating; Further stages.;		68%

Cyclohexyl-phenylsulfanylmethyl-amine; hydrochloride

100-60-7

N-methylcyclohexylamine

Conditions
ConditionsYield
With lithium aluminium tetrahydride In diethyl ether -60 degC -> room temp.;67%

N-Methylcyclohexylamine Chemical Properties

MF: C7H15N
MW: 113.2
EINECS: 202-869-3
mp  -9 ~ -7 °C(lit.)
bp  149 °C(lit.)
density  0.868 g/mL at 25 °C(lit.)
vapor density  4 (vs air)
vapor pressure  11 mm Hg ( 40 °C)
refractive index  n20/D 1.456(lit.)
Fp  85 °F
storage temp.  Flammables area
Water Solubility  5.4 g/100 mL (20 oC)
Sensitive  Air Sensitive

N-Methylcyclohexylamine Toxicity Data With Reference

RTECS  GX1529000

N-Methylcyclohexylamine Safety Profile

Hazard Codes  C
Risk Statements  10-21/22-35-20/21/22
Safety Statements  16-26-36/37/39-45
RIDADR  UN 2734 8/PG 2
WGK Germany  1
Hazard Note  Corrosive
HazardClass  8
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