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Name |
N-phenylglycine |
EINECS | 203-070-2 |
CAS No. | 103-01-5 | Density | 1.259 g/cm3 |
PSA | 49.33000 | LogP | 1.25610 |
Solubility | moderately soluble in water | Melting Point |
121-127 °C |
Formula | C8H9NO2 | Boiling Point | 359 °C at 760 mmHg |
Molecular Weight | 151.165 | Flash Point | 170.9 °C |
Transport Information | N/A | Appearance | ochre to yellow-brown fine powder |
Safety | 22-24/25 | Risk Codes | 36/37/38 |
Molecular Structure | Hazard Symbols | N/A | |
Synonyms |
H-DL-Phg-OH;TR-NPG;(Phenylamino)aceticacid;Acetic acid, (phenylamino)-;Anilinoacetic acid;N-(Phenylamino)aceticacid;N-Phenylglycine;NSC 83567; |
Article Data | 101 |
Conditions | Yield |
---|---|
Stage #1: ethyl bromoacetate; aniline With silica gel at 20℃; for 0.116667h; microwave irradiation; Stage #2: With sodium hydroxide In ethanol for 0.166667h; Heating; | 93% |
Stage #1: ethyl bromoacetate; aniline With potassium carbonate for 1.5h; Milling; Stage #2: With potassium hydroxide for 1.5h; Milling; | 91% |
Stage #1: ethyl bromoacetate; aniline Stage #2: With sodium hydroxide |
Conditions | Yield |
---|---|
90% |
tert-butyl 2-(phenylamino)acetate
N-Phenylglycine
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane for 3h; | 90% |
In water; isopropyl alcohol at 200℃; for 0.25h; Solvent; Temperature; Flow reactor; | 77% |
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; 2-(N,N-dimethylamino)ethanol In water at 75 - 80℃; for 72h; | 87% |
With copper(l) iodide; 2-(2-methyl-1-oxopropyl)cyclohexanone; caesium carbonate In N,N-dimethyl-formamide at 20℃; for 4h; Inert atmosphere; | 82% |
With copper(I) oxide; caesium carbonate at 100℃; for 0.666667h; Sealed tube; Microwave irradiation; | 10% |
Conditions | Yield |
---|---|
With copper(l) iodide; 2-(2-methyl-1-oxopropyl)cyclohexanone; potassium carbonate In water at 90℃; for 0.833333h; Microwave irradiation; Green chemistry; | 81% |
With pectin-stabilized copper nanoparticles In dimethyl sulfoxide at 110℃; for 2h; | 71% |
With potassium phosphate; copper(l) iodide; 2-(N,N-dimethylamino)ethanol In water at 90℃; | 62% |
With copper(l) iodide; potassium carbonate In N,N-dimethyl acetamide at 90℃; |
Conditions | Yield |
---|---|
With sodium hydroxide In water for 0.5h; Heating; | 73% |
With sodium hydroxide for 0.5h; Heating; | 70% |
Stage #1: N-phenylglycine ethyl ester With sodium hydroxide In water for 0.5h; Reflux; Stage #2: With hydrogenchloride In water pH=2; |
1-phenyl-4-oximinoimidazolidine
N-Phenylglycine
Conditions | Yield |
---|---|
With hydrogenchloride Hydrolysis; | 60% |
iodobenzene
glycylglycine
A
N-(N-phenyl-glycyl)-glycine
B
N-Phenylglycine
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; 2-(N,N-dimethylamino)ethanol In water at 70℃; for 16h; | A 40% B 27% |
Conditions | Yield |
---|---|
With sulfuric acid Electrolysis.elektrolytische Reduktion; |
Conditions | Yield |
---|---|
With potassium cyanide; ethanol |