Phosphorodifluoridic acid, lithium salt

There total 3 articles about Phosphorodifluoridic acid, lithium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

Reference yield:

21324-40-3

lithium hexafluorophosphate

554-13-2

lithium carbonate

24389-25-1

difluorophosphinic acid lithium salt

Guidance literature:

at 65 ℃; for 12h; Temperature; Inert atmosphere; Glovebox;

DOI:10.1016/j.cclet.2020.05.006

Reference yield:

14456-60-1

difluorophosphoric acid anhydride

7789-24-4

lithium fluoride

24389-25-1

difluorophosphinic acid lithium salt

Guidance literature:

In neat (no solvent); byproducts: POF3; LiF was added to P2O3F4 at -0.1°C, warmed to ambient temp.; evapd. at 100-120°C;

DOI:10.1016/0584-8539(82)80068-8

Reference yield:

hexafluorophosphoric acid

16752-60-6

phosphorus pentoxide

7789-24-4

lithium fluoride

24389-25-1

difluorophosphinic acid lithium salt

Guidance literature:

at 220 ℃; for 122h; Autoclave;

DOI:10.1039/c8cc10158b