4,4'-Dihexylazoxybenzene

Base Information

• Chemical Name: 4,4'-Dihexylazoxybenzene
• CAS No.: 37592-88-4
• Molecular Formula: C₂₄H₃₄N₂O
• Molecular Weight: 366.547
• Mol file: 37592-88-4.mol

Synonyms:4,4'-Dihexylazoxybenzene;37592-88-4;(4-hexylphenyl)-(4-hexylphenyl)imino-oxidoazanium;MFCD00043688;AKOS015839933;(Z)-1,2-bis(4-hexylphenyl)diazene oxide;FT-0617055

Chemical Property of 4,4'-Dihexylazoxybenzene

Chemical Property:

• Boiling Point: 493.4oC at 760 mmHg
• Flash Point: >230 °F
• PSA: 41.11000
• Density: 0.98g/cm3
• LogP: 8.38110
• XLogP3: 9.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 12
• Exact Mass: 366.267113712
• Heavy Atom Count: 27
• Complexity: 393

Purity/Quality:

98%Min ^*data from raw suppliers

4,4'-Dihexylazoxybenzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCC1=CC=C(C=C1)N=[N+](C2=CC=C(C=C2)CCCCCC)[O-]

Technology Process of 4,4'-Dihexylazoxybenzene

There total 4 articles about 4,4'-Dihexylazoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

4-hexylaniline (33228-45-4) → 1,2-bis(4-hexylphenyl)diazene oxide (37592-88-4,95856-89-6)

Guidance literature:

With 2,2,2-Trifluoroacetophenone; dihydrogen peroxide; acetonitrile; In ethanol; at 20 ℃; for 18h; Green chemistry;

DOI:10.1039/c6gc03174a

Reference yield:

→ 4,4'-bis(hexyl)azoxybenzene (37592-88-4,95856-89-6)

Guidance literature:

Reference yield:

→ 1,2-bis(4-hexylphenyl)diazene oxide (37592-88-4,95856-89-6)

Guidance literature:

durch Oxid. des entspr. Anilins;

upstream raw materials:

4-hexylaniline

Refernces

• 1、 -. "Process for preparing 2,3-dihydro-1,3-dialkyl-2,3-dialkyl perimidines and N,N-'-dialkyl-1,8-naphthalene diamines". . . Retrieved 2008/06/13.