2,2'-Thiobis(4-Methylphenol)

Base Information

• Chemical Name: 2,2'-Thiobis(4-Methylphenol)
• CAS No.: 2929-96-6
• Molecular Formula: C14H14O2S
• Molecular Weight: 246.33
• Mol file: 2929-96-6.mol

Synonyms:5-methyl-2-hydroxyphenyl sulfide;4,4''-Dimethyl-2,2''-sulfandiyl-di-phenol;4,4''-Sulfonyldibenzylalkohol;2,2'-THIOBIS(4-METHYLPHENOL);Phenol, 2,2‘-thiobis[4-methyl-;

Chemical Property of 2,2'-Thiobis(4-Methylphenol)

Chemical Property:

• PSA: 65.76000
• LogP: 3.86580

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,2'-Thiobis(4-Methylphenol)

There total 6 articles about 2,2'-Thiobis(4-Methylphenol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-(2-hydroxy-5-methylphenylsulfinyl)-4-methylphenol (27725-15-1) → 2,2'-thiobis<4-methylphenol> (2929-96-6)

Guidance literature:

With silica gel; acetic acid; zinc; for 0.0833333h; microwave irradiation;

DOI:10.1080/714040965

Reference yield: 65.0%

p-cresol (106-44-5) → 2,2'-thiobis<4-methylphenol> (2929-96-6)

Guidance literature:

With sulfur dichloride; In Petroleum ether; at 20 ℃;

DOI:10.1080/10426500600619484

Reference yield: 61.0%

p-cresol (106-44-5) → 2,2'-thiobis<4-methylphenol> (2929-96-6) + 2,6-bis(2-hydroxy-5-methylphenylthio)-4-methylphenol (133786-57-9)

Guidance literature:

With sulfur dichloride; In dichloromethane;

DOI:10.1246/bcsj.64.576

upstream raw materials:

p-cresol

2-(2-hydroxy-5-methylphenylsulfinyl)-4-methylphenol

C₁₄H₁₂O₂S

Downstream raw materials:

bis-(2-acetoxy-5-methyl-phenyl)-sulfide

3-(2-hydroxy-5-methylphenylthio)-2-hydroxy-5-methylbenzyl alcohol

3,3'-thiobis<2-hydroxy-5-methylbenzenemethanol>

2-<3-<3-(3-bromo-5-methylsalicyl)-5-methylsalicyl>-2-hydroxy-5-methylphenylthio>-4-methylphenol