1H-IMidazole,2-(broMoMethyl)-,hydrobroMide(1:1)

Base Information

• Chemical Name: 1H-IMidazole,2-(broMoMethyl)-,hydrobroMide(1:1)
• CAS No.: 2939-05-1
• Molecular Formula: C4H5BrN2.BrH
• Molecular Weight: 241.91200
• Mol file: 2939-05-1.mol

Synonyms:1H-Imidazole, 2-(bromomethyl)-, monohydrobromide (9CI);1H-Imidazole, 2-(bromomethyl)-, hydrobromide (1:1);Imidazole, 2-(bromomethyl)-, hydrobromide (7CI,8CI);

Chemical Property of 1H-IMidazole,2-(broMoMethyl)-,hydrobroMide(1:1)

Chemical Property:

• PSA: 28.68000
• LogP: 2.26270
• Storage Temp.: Inert atmosphere,Store in freezer, under -20°C

Purity/Quality:

97% ^*data from raw suppliers

2-(Bromomethyl)-1H-imidazolehydrobromide 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 1H-IMidazole,2-(broMoMethyl)-,hydrobroMide(1:1)

There total 1 articles about 1H-IMidazole,2-(broMoMethyl)-,hydrobroMide(1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

2-hydroxymethyl-1H-imidazole (3724-26-3) → 2-(bromomethyl)-1H-imidazole hydrobromide (2939-05-1)

Guidance literature:

With hydrogen bromide; In acetic acid; at 100 ℃; for 5h;

DOI:10.1021/acs.jmedchem.0c01856

Reference yield: 57.0%

2-(bromomethyl)-1H-imidazole hydrobromide (2939-05-1) + 2-amino-6-sulfanyl-4-phenylnicotinonitrile → 6-(((1H-imidazol-2-yl)methyl)thio)-2-amino-4-phenylnicotinonitrile

Guidance literature:

With sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 50 ℃; for 4h;

DOI:10.1021/acs.jmedchem.0c01856

Reference yield: 46.0%

2-(bromomethyl)-1H-imidazole hydrobromide (2939-05-1) + 2-amino-4-sulfanyl-6-phenylpyrimidine-5-carbonitrile → 4-((1H-imidazol-2-yl)methylthio)-2-amino-6-phenylpyrimidine-5-carbonitrile

Guidance literature:

With sodium carbonate; In N,N-dimethyl-formamide; for 4h;

DOI:10.1021/acs.jmedchem.0c01856

upstream raw materials:

2-hydroxymethyl-1H-imidazole

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