[CeCl₄(triphenylphosphine oxide)2]

Base Information

• Chemical Name: [CeCl₄(triphenylphosphine oxide)2]
• CAS No.: 33989-88-7
• Molecular Formula: C₃₆H₃₀CeCl₄O₂P₂
• Molecular Weight: 838.513

Synonyms:

Chemical Property of [CeCl₄(triphenylphosphine oxide)2]

Chemical Property:

Purity/Quality:

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Technology Process of [CeCl₄(triphenylphosphine oxide)2]

There total 1 articles about [CeCl₄(triphenylphosphine oxide)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

H2CeCl6(diethylene glycol dimethyl ether)3 + Triphenylphosphine oxide (791-28-6) → [CeCl4(triphenylphosphine oxide)2] (33989-88-7)

Guidance literature:

In methanol; dichloromethane; ethyl acetate; soln. of Ce-complex in ethyl acetate-MeOH was cooled in ice, stirred for 5 min, centrifuged, decanted, CH2Cl2 soln. of ligand in 5-10% excess was slowly added; ether added dropwise to turbidity, left in ice for crystn., supernatantliq. decanted, crystals washed with ether, vac. dried at room temp.; elem. anal.;

DOI:10.1039/DT9830001265

upstream raw materials:

Triphenylphosphine oxide

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