NCC₆H₄CB₁₀H₁₀CCH₂OSi(CH₃)2C(CH₃)3

Base Information

Chemical Name:NCC₆H₄CB₁₀H₁₀CCH₂OSi(CH₃)2C(CH₃)3
CAS No.:862467-04-7
Molecular Formula:C₁₆H₃₁B₁₀NOSi
Molecular Weight:389.624
Hs Code.:

NCC<sub>6</sub>H<sub>4</sub>CB<sub>10</sub>H<sub>10</sub>CCH<sub>2</sub>OSi(CH<sub>3</sub>)2C(CH<sub>3</sub>)3

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of NCC₆H₄CB₁₀H₁₀CCH₂OSi(CH₃)2C(CH₃)3

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Technology Process of NCC₆H₄CB₁₀H₁₀CCH₂OSi(CH₃)2C(CH₃)3

There total 1 articles about NCC₆H₄CB₁₀H₁₀CCH₂OSi(CH₃)2C(CH₃)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 862466-81-7
tert-butyldimethylsilyoxymethyl-p-carborane

: 69113-59-3
3-iodobenzonitrile

: 862467-04-7
NCC₆H₄CB₁₀H₁₀CCH₂OSi(CH₃)2C(CH₃)3

Guidance literature:: With pyridine; n-butyllithium; copper(l) chloride; In 1,2-dimethoxyethane; hexane; to soln. p-carborane in DME soln. n-BuLi in hexane was added at 0°C under Ar and stirred for 30 min, CuCl was added and stirred at room temp. for 2 h, pyridine and 3-NCC6H4I were added and refluxed for 4 h; react. mixt. was cooled, soln. was filtered, washed with 2 N HCl, water,and brine, dried over MgSO4 and concd., chromy. on silica (EtOAc-n-hexa ne 1:10);
DOI:10.1021/ic0509736