Cyclohexene, 1,1'-(1,3-butadiyne-1,4-diyl)bis-

Base Information

• Chemical Name: Cyclohexene, 1,1'-(1,3-butadiyne-1,4-diyl)bis-
• CAS No.: 2979-05-7
• Molecular Formula: C16H18
• Molecular Weight: 210.319
• Mol file: 2979-05-7.mol

Synonyms:

Chemical Property of Cyclohexene, 1,1'-(1,3-butadiyne-1,4-diyl)bis-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Cyclohexene, 1,1'-(1,3-butadiyne-1,4-diyl)bis-

There total 25 articles about Cyclohexene, 1,1'-(1,3-butadiyne-1,4-diyl)bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

1-ethenylcyclohexene (931-49-7) → di-cyclohex-1-enyl-butadiyne (2979-05-7)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; air; palladium diacetate; copper(l) iodide; In acetonitrile; at 20 ℃; for 3h;

DOI:10.1021/jo0503310

Reference yield: 90.0%

C42H42P2Pd → di-cyclohex-1-enyl-butadiyne (2979-05-7)

Guidance literature:

In [⁽²⁾H₆]acetone; at 9.84 ℃; for 13h;

DOI:10.1021/acscatal.8b01540

Reference yield: 87.0%

1-ethenylcyclohexene (931-49-7) + benzyl azide (622-79-7) → 1-benzyl-4-(cyclohex-1-en-1-yl)-1H-1,2,3-triazole + di-cyclohex-1-enyl-butadiyne (2979-05-7)

Guidance literature:

With Cu₂(OH)3OAc*H₂O; In acetonitrile; at 100 ℃; for 0.166667h; Microwave irradiation;

DOI:10.1039/b924649e

upstream raw materials:

1,4-bis(1-hydroxycyclohexyl)buta-1,3-diyne

1-ethenylcyclohexene

(Cyclohex-1-enylethynylselanyl)-benzene

2-triethylsilylacetylene

Downstream raw materials:

2,5-di(cyclohex-1-enyl)thiophene