Benzenemethanol, a-ethynyl-3-methyl-

Base Information

Chemical Name:Benzenemethanol, a-ethynyl-3-methyl-
CAS No.:29978-38-9
Molecular Formula:C10H10O
Molecular Weight:146.189
Hs Code.:
Mol file:29978-38-9.mol

Synonyms:1-(3-methylphenyl)-2-propyn-1-ol;1-(m-tolyl)prop-2-yn-1-ol;1-m-tolylprop-2-yn-1-ol;1-(m-tolyl)-2-propyn-1-ol;

Suppliers and Price of Benzenemethanol, a-ethynyl-3-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chemenu
1-(3-Methylphenyl)-2-propyn-1-ol 95%
5g
$ 649.00

AK Scientific
1-(m-Methylphenyl)-2-propyn-1-ol
5g
$ 863.00

Total 4 raw suppliers

Chemical Property of Benzenemethanol, a-ethynyl-3-methyl-

Chemical Property:

PSA：20.23000
LogP:1.66160

Purity/Quality:

97% ^*data from raw suppliers

1-(3-Methylphenyl)-2-propyn-1-ol 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenemethanol, a-ethynyl-3-methyl-

There total 7 articles about Benzenemethanol, a-ethynyl-3-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 620-23-5
m-tolyl aldehyde

: 4301-14-8
acetylenemagnesium bromide

: 29978-38-9
1-(m-tolyl)prop-2-yn-1-ol

Guidance literature:: at -78 - 0 ℃; Yield given;
DOI:10.1016/0957-4166(96)00166-8

Reference yield:

: 1310487-12-7,1310487-25-2
1-(m-tolyl)-3-(trimethylsilyl)prop-2-yn-1-ol

: 29978-38-9
1-(m-tolyl)prop-2-yn-1-ol

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; Inert atmosphere;
DOI:10.1002/adsc.201000833

Reference yield:

: 620-23-5
m-tolyl aldehyde

: 1066-54-2
trimethylsilylacetylene

: 29978-38-9
1-(m-tolyl)prop-2-yn-1-ol

Guidance literature:: trimethylsilylacetylene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

m-tolyl aldehyde; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

With water; sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol901891u