Ethanol, 2-[ethyl[4-(phenylazo)phenyl]amino]-

Base Information

• Chemical Name: Ethanol, 2-[ethyl[4-(phenylazo)phenyl]amino]-
• CAS No.: 3009-45-8
• Molecular Formula: C16H19N3O
• Molecular Weight: 269.346
• Hs Code.: 2927000090
• European Community (EC) Number: 608-442-1
• DSSTox Substance ID: DTXSID90548901
• Nikkaji Number: J70.267F
• Mol file: 3009-45-8.mol

Synonyms:3009-45-8;Ethanol, 2-[ethyl[4-(phenylazo)phenyl]amino]-;2-(N-ethyl-4-phenyldiazenylanilino)ethanol;Ethanol, 2-[ethyl[4-(2-phenyldiazenyl)phenyl]aMino]-;SCHEMBL4637916;DTXSID90548901;GHGOCLGPGNHCBX-UHFFFAOYSA-N;N-ethyl-N-(2-hydroxyethyl)-4-phenylazoaniline;2-(Ethyl{4-[(E)-phenyldiazenyl]phenyl}amino)ethan-1-ol

Chemical Property of Ethanol, 2-[ethyl[4-(phenylazo)phenyl]amino]-

Chemical Property:

• Vapor Pressure: 5.42E-09mmHg at 25°C
• Boiling Point: 452.9oC at 760 mmHg
• Flash Point: 227.7oC
• PSA: 48.19000
• Density: 1.07g/cm3
• LogP: 3.92060
• XLogP3: 3.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 6
• Exact Mass: 269.152812238
• Heavy Atom Count: 20
• Complexity: 281

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN(CCO)C1=CC=C(C=C1)N=NC2=CC=CC=C2

Technology Process of Ethanol, 2-[ethyl[4-(phenylazo)phenyl]amino]-

There total 2 articles about Ethanol, 2-[ethyl[4-(phenylazo)phenyl]amino]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

2-( N-ethylanilino)ethanol (92-50-2) + aniline (62-53-3) → 4'-<2-((hydroxy)ethyl)ethylamino>azobenzene (3009-45-8)

Guidance literature:

aniline; With hydrogenchloride; sodium nitrite; In water; at 0 ℃; for 0.25h;

2-( N-ethylanilino)ethanol; With acetic acid; In water; for 0.0833333h;

DOI:10.1039/c8ra01660g

Reference yield:

→ 4'-<2-((hydroxy)ethyl)ethylamino>azobenzene (3009-45-8)

Guidance literature:

/BRN= 3389285/;

Reference yield: 100.0%

6-O-(3-carboxypropanoyl)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose (119613-87-5) + 4'-<2-((hydroxy)ethyl)ethylamino>azobenzene (3009-45-8) → 2-[ethyl-(4'-phenylazo-phenyl)-amino]ethyl 1,2:3,4-di-O-isopropylidengalactose-6-succinate (764661-91-8)

Guidance literature:

With 2-(Dimethylamino)pyridine; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In tetrahydrofuran; at 20 ℃; for 16h;

upstream raw materials:

2-( N-ethylanilino)ethanol

aniline

Downstream raw materials:

succinic acid 5-(2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester 2-[ethyl-(4-phenylazo-phenyl)-amino]-ethyl ester

2-[ethyl-(4'-phenylazo-phenyl)-amino]ethyl 1,2:3,4-di-O-isopropylidengalactose-6-succinate

succinic acid 7-acetoxy-6-[(5-dimethoxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-(2,2-dimethyl-[1,3]dioxolan-4-yl)-methoxy]-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-4-ylmethyl ester 2-[ethyl-(4-phenylazo-phenyl)-amino]-ethyl ester

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