o-nitrophenyl S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->4)-S-(2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranoside

Base Information

• Chemical Name: o-nitrophenyl S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->4)-S-(2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranoside
• CAS No.: 93677-32-8
• Molecular Formula: C₄₄H₅₅NO₂₆S₂
• Molecular Weight: 1078.04

Synonyms:

Chemical Property of o-nitrophenyl S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->4)-S-(2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranoside

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

Technology Process of o-nitrophenyl S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->4)-S-(2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranoside

There total 1 articles about o-nitrophenyl S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->4)-S-(2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetic anhydride (108-24-7) + o-nitrophenyl S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->4)-S-(2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-4-thio-α-D-glucopyranoside (93677-31-7) → o-nitrophenyl S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->4)-S-(2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranoside (93677-32-8)

Guidance literature:

With pyridine; sodium methylate; Yield given. Multistep reaction; 1.) methanol, 78 h;

DOI:10.1039/P19840001885

Reference yield:

o-nitrophenyl S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->4)-S-(2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranoside (93677-32-8) → o-nitrophenyl 4,4'-dithio-α-maltotrioside (93677-33-9)

Guidance literature:

With Amberlite IR 120 (H+); sodium methylate; Yield given. Multistep reaction; 1.) methanol;

DOI:10.1039/P19840001885

upstream raw materials:

acetic anhydride

o-nitrophenyl S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->4)-S-(2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-4-thio-α-D-glucopyranoside

Downstream raw materials:

o-nitrophenyl 4,4'-dithio-α-maltotrioside

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