tetraethylammonium tricarbonyl-1,1,1-tris(diphenylphosphinomethyl)ethanevanadate(-I)

Base Information

Chemical Name:tetraethylammonium tricarbonyl-1,1,1-tris(diphenylphosphinomethyl)ethanevanadate(-I)
CAS No.:73299-93-1
Molecular Formula:C₈H₂₀N*C₄₄H₃₉O₃P₃V
Molecular Weight:889.908
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetraethylammonium tricarbonyl-1,1,1-tris(diphenylphosphinomethyl)ethanevanadate(-I)

Chemical Property:

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Technology Process of tetraethylammonium tricarbonyl-1,1,1-tris(diphenylphosphinomethyl)ethanevanadate(-I)

There total 1 articles about tetraethylammonium tricarbonyl-1,1,1-tris(diphenylphosphinomethyl)ethanevanadate(-I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13985-78-9
tetraethylammonium hexacarbonylvanadium(-1)

: 22031-12-5
[2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine]

: 60479-89-2
cis-tetraethylammonium tetracarbonyl-1,1,1-tris(diphenylphosphinomethyl)ethanevanadate(-I)

: 73299-93-1
tetraethylammonium tricarbonyl-1,1,1-tris(diphenylphosphinomethyl)ethanevanadate(-I)

Guidance literature:: In tetrahydrofuran; Irradiation (UV/VIS); (N2); soln. or V-complex and phosphine deriv. was irradiated for 5,5 h; formed ppt. of V(CO)4-compd. was sepd., washed with THF and crystd. from MeCN/THF on standing for 5 d at 273 K; elem. anal.; filtrate of ppt. was allowed to stand for several d at 273 K, formed black plates were sepd. and dried in vac.; elem. anal.;
DOI:10.1016/S0022-328X(00)93761-6

Reference yield:

: 73299-93-1
tetraethylammonium tricarbonyl-1,1,1-tris(diphenylphosphinomethyl)ethanevanadate(-I)

: bis(bromodinitrosylcobalt)

: 82887-75-0
V(CO)2(NO)(CH₃C(CH₂P(C₆H₅)2)3)

Guidance literature:: In tetrahydrofuran; acetonitrile; byproducts: N(C2H5)4Br, Co(CO)3NO; to frozen (liquid air) soln. of V complex in mixt. of MeCN and THF added soln. of (Co(NO)2Br)2 in THF, gradually warmed to room temp., stirred for 1 h; evapd. in vac., added THF, filtered NEt4Br, ppt. by addn. of hexane, recrystd. from THF/heptane; elem. anal.;
DOI:10.1016/S0022-328X(00)89065-8