Molybdenum, tetrachlorobis(methyldiphenylphosphine)-

Base Information

Chemical Name:Molybdenum, tetrachlorobis(methyldiphenylphosphine)-
CAS No.:30411-57-5
Molecular Formula:C₂₆H₂₆Cl₄MoP₂
Molecular Weight:638.192
Hs Code.:

Synonyms:

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Chemical Property of Molybdenum, tetrachlorobis(methyldiphenylphosphine)-

Chemical Property:

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Technology Process of Molybdenum, tetrachlorobis(methyldiphenylphosphine)-

There total 1 articles about Molybdenum, tetrachlorobis(methyldiphenylphosphine)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 144299-52-5,58904-33-9,58918-77-7
Mo(P(CH₃)(C₆H₅)2)3Cl₃

: 144299-53-6,32025-94-8
ReCl₄(PMePh₂)2

: 23136-99-4,80656-01-5
ReCl₃(PMePh₂)₃

: 30411-57-5,30059-53-1
tetrachlorobis(methyldiphenylphosphine)molybdenum(IV)

Guidance literature:: In benzene-d6; (N2 or Ar); react. in a C6D6 soln. at 25°C in an evacuated and flame-sealed NMR tube; monitored by (1)H and (31)P NMR;

Reference yield: 55.0%

: 30411-57-5,30059-53-1
tetrachlorobis(methyldiphenylphosphine)molybdenum(IV)

: 1486-28-8
diphenyl(methyl)phosphine

: Mo(P(CH₃)(C₆H₅)2)4Cl₂

Guidance literature:: With magnesium; In tetrahydrofuran; under protective gas, THF condensed to a mixture of Mo-compd. and Mg, warmed to room temp., PMePh2 added via a syringe, stirred for 3 h; filtered, evapd., toluene added, filtered, evapd., dissolved in toluene, concd., cooled slowly to -15°C, pptd with pentane, filtered, washed with Et2O, dried, stirred in pentane for few h, filtered, dried in vac. overnight, elem. anal.;

Reference yield:

: 90245-62-8,146142-77-0
WCl₂(PMePh₂)4

: 30411-57-5,30059-53-1
tetrachlorobis(methyldiphenylphosphine)molybdenum(IV)

: 75598-29-7,36151-19-6
W^IVCl₄(PMePh₂)2

Guidance literature:: In benzene-d6; (N2 or Ar); react. in a C6D6 soln. at 25°C in an evacuated and flame-sealed NMR tube; monitored by (1)H and (31)P NMR;