N₈,N₈,N₂₀,N₂₀-Tetraethyl-2,2,14,14-tetramethyl-7,9,19,21-tetraoxa-8,20-diphosphapentacyclo-[20.2.2.2^3,6.2^10,13.2^15,18]dotriaconta-1⁽²⁴⁾,3,5,10,12,15,17,22,25,27,29,31-dodecaen-8,20-diamin

Base Information

• Chemical Name: N₈,N₈,N₂₀,N₂₀-Tetraethyl-2,2,14,14-tetramethyl-7,9,19,21-tetraoxa-8,20-diphosphapentacyclo-[20.2.2.2^3,6.2^10,13.2^15,18]dotriaconta-1⁽²⁴⁾,3,5,10,12,15,17,22,25,27,29,31-dodecaen-8,20-diamin
• CAS No.: 272460-92-1
• Molecular Formula: C₃₈H₄₈N₂O₄P₂
• Molecular Weight: 658.758

Synonyms:

Chemical Property of N₈,N₈,N₂₀,N₂₀-Tetraethyl-2,2,14,14-tetramethyl-7,9,19,21-tetraoxa-8,20-diphosphapentacyclo-[20.2.2.2^3,6.2^10,13.2^15,18]dotriaconta-1⁽²⁴⁾,3,5,10,12,15,17,22,25,27,29,31-dodecaen-8,20-diamin

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Technology Process of N₈,N₈,N₂₀,N₂₀-Tetraethyl-2,2,14,14-tetramethyl-7,9,19,21-tetraoxa-8,20-diphosphapentacyclo-[20.2.2.2^3,6.2^10,13.2^15,18]dotriaconta-1⁽²⁴⁾,3,5,10,12,15,17,22,25,27,29,31-dodecaen-8,20-diamin

There total 1 articles about N₈,N₈,N₂₀,N₂₀-Tetraethyl-2,2,14,14-tetramethyl-7,9,19,21-tetraoxa-8,20-diphosphapentacyclo-[20.2.2.2^3,6.2^10,13.2^15,18]dotriaconta-1⁽²⁴⁾,3,5,10,12,15,17,22,25,27,29,31-dodecaen-8,20-diamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

BPA (80-05-7) + N,N,N',N'-Tetraethyl-[4-(1-{4-[1-(4-{[1,1-bis(diethylamino)phosphino]oxy}-3,5-dimethylphenyl)-1-methylethyl]phenyl}-1-methylethyl)-2,6-dimethylphenyl]-phosphordiamidit (272460-91-0) → N8,N8,N20,N20-Tetraethyl-2,2,14,14-tetramethyl-7,9,19,21-tetraoxa-8,20-diphosphapentacyclo-[20.2.2.23,6.210,13.215,18]dotriaconta-1(24),3,5,10,12,15,17,22,25,27,29,31-dodecaen-8,20-diamin (272460-92-1) + rac-(+/-)-N,N-Diethyl-[4-(1-{4-[1-(4-hydroxy-3,5-dimethylphenyl)-1-methylethyl]phenyl}-1-methylethyl)-2,6-dimethylphenyl]-4-[1-(4-hydroxyphenyl)-1-methyl-ethyl]phenyl-phosphoramidit

Guidance literature:

In toluene; for 24h; Heating;

DOI:10.1080/10426509808045481

upstream raw materials:

BPA

N,N,N',N'-Tetraethyl-[4-(1-{4-[1-(4-{[1,1-bis(diethylamino)phosphino]oxy}-3,5-dimethylphenyl)-1-methylethyl]phenyl}-1-methylethyl)-2,6-dimethylphenyl]-phosphordiamidit

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