(Re(CO)4)2(C₁₂H₂₅OC₆H₃CHNC₆H₄)2COO

Base Information

• Chemical Name: (Re(CO)4)2(C₁₂H₂₅OC₆H₃CHNC₆H₄)2COO
• CAS No.: 284038-01-3
• Molecular Formula: C₅₉H₆₆N₂O₁₂Re₂
• Molecular Weight: 1367.59

Synonyms:

Chemical Property of (Re(CO)4)2(C₁₂H₂₅OC₆H₃CHNC₆H₄)2COO

Chemical Property:

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Technology Process of (Re(CO)4)2(C₁₂H₂₅OC₆H₃CHNC₆H₄)2COO

There total 1 articles about (Re(CO)4)2(C₁₂H₂₅OC₆H₃CHNC₆H₄)2COO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pentacarbonylmethylrhenium(I) (14524-92-6) + 4-{[(E)-4-Dodecyloxy-phenylimino]-methyl}-benzoic acid 4-{[(E)-4-dodecyloxy-phenylimino]-methyl}-phenyl ester → (Re(CO)4)2(C12H25OC6H3CHNC6H4)2COO (284038-01-3)

Guidance literature:

In toluene; to suspn. of ligand in toluene was added Re-complex, mixt. was stirred under reflux for 20 h under N2, cooled to room temp.; solvent was removed, dissolved in CH2Cl2, column chromy. (alumina, CH2Cl2), concd., hexane was added; elem. anal.;

DOI:10.1039/a910273f

upstream raw materials:

pentacarbonylmethylrhenium(I)

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