L-Phenylalanine,5-[(1Z)-2-aminoethenyl]-2-methoxy-N-methyl-D-phenylalanyl-L-isoleucyl-, (3®1)-lactam(9CI)

Base Information

Chemical Name:L-Phenylalanine,5-[(1Z)-2-aminoethenyl]-2-methoxy-N-methyl-D-phenylalanyl-L-isoleucyl-, (3®1)-lactam(9CI)
CAS No.:84173-39-7
Molecular Formula:C₂₈H₃₆N₄O₄
Molecular Weight:492.618
Hs Code.:

Synonyms:4,7,10-Triazabicyclo[12.3.1]octadeca-1(18),2,14,16-tetraene-5,8,11-trione,15-methoxy-12-(methylamino)-9-(1-methylpropyl)-6-(phenylmethyl)-,[6S-[2Z,6R*,9R*(R*),12S*]]-; Isomucronine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of L-Phenylalanine,5-[(1Z)-2-aminoethenyl]-2-methoxy-N-methyl-D-phenylalanyl-L-isoleucyl-, (3®1)-lactam(9CI)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of L-Phenylalanine,5-[(1Z)-2-aminoethenyl]-2-methoxy-N-methyl-D-phenylalanyl-L-isoleucyl-, (3®1)-lactam(9CI)

There total 22 articles about L-Phenylalanine,5-[(1Z)-2-aminoethenyl]-2-methoxy-N-methyl-D-phenylalanyl-L-isoleucyl-, (3®1)-lactam(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54793-60-1
H-(S)-Ile-(S)-Phe-OCH₃

: 38840-26-5,84173-39-7
Mucronin B

Guidance literature:: Multi-step reaction with 7 steps

1: 1) NaOH, 2) DCCD / 1) H₂O/dioxane, r.t., 4h, 2) CH₂Cl₂, 0 deg C, 10h

2: NaOH / H₂O; dioxane / 4 h / Ambient temperature

3: DCCD / CH₂Cl₂ / 10 h / 0 °C

4: 85 percent / H₂ / Pd / dioxane / 5 h / 95 °C

5: pyridine / 20 h / Ambient temperature

6: trifluoroacetic acid / 20 h / 50 °C

7: NaIO₄ / tetrahydrofuran; methanol; H₂O / 0.5 h / Ambient temperature

With sodium hydroxide; sodium periodate; hydrogen; dicyclohexyl-carbodiimide; palladium; In tetrahydrofuran; 1,4-dioxane; pyridine; methanol; dichloromethane; water; trifluoroacetic acid;

Reference yield:

: 84133-16-4
(S)-2-{(2S,3S)-2-[3-[5-(2-Benzyloxycarbonylamino-1-hydroxy-ethyl)-2-methoxy-phenyl]-2-(tert-butoxycarbonyl-methyl-amino)-propionylamino]-3-methyl-pentanoylamino}-3-phenyl-propionic acid

: 38840-26-5,84173-39-7
Mucronin B

Guidance literature:: Multi-step reaction with 5 steps

1: DCCD / CH₂Cl₂ / 10 h / 0 °C

2: 85 percent / H₂ / Pd / dioxane / 5 h / 95 °C

3: pyridine / 20 h / Ambient temperature

4: trifluoroacetic acid / 20 h / 50 °C

5: NaIO₄ / tetrahydrofuran; methanol; H₂O / 0.5 h / Ambient temperature

With sodium periodate; hydrogen; dicyclohexyl-carbodiimide; palladium; In tetrahydrofuran; 1,4-dioxane; pyridine; methanol; dichloromethane; water; trifluoroacetic acid;

Reference yield:

: 84133-17-5
(S)-2-{(2S,3S)-2-[3-[5-(2-Benzyloxycarbonylamino-1-hydroxy-ethyl)-2-methoxy-phenyl]-2-(tert-butoxycarbonyl-methyl-amino)-propionylamino]-3-methyl-pentanoylamino}-3-phenyl-propionic acid pentafluorophenyl ester

: 38840-26-5,84173-39-7
Mucronin B

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / H₂ / Pd / dioxane / 5 h / 95 °C

2: pyridine / 20 h / Ambient temperature

3: trifluoroacetic acid / 20 h / 50 °C

4: NaIO₄ / tetrahydrofuran; methanol; H₂O / 0.5 h / Ambient temperature

With sodium periodate; hydrogen; palladium; In tetrahydrofuran; 1,4-dioxane; pyridine; methanol; water; trifluoroacetic acid;