[1,1'-Biphenyl]-4-ol, 4'-[(4-chlorophenyl)sulfonyl]-

Base Information

Chemical Name:[1,1'-Biphenyl]-4-ol, 4'-[(4-chlorophenyl)sulfonyl]-
CAS No.:30809-75-7
Molecular Formula:C18H13ClO3S
Molecular Weight:344.818
Hs Code.:
DSSTox Substance ID:DTXSID00440169
Nikkaji Number:J606.118D
Wikidata:Q82256407
Mol file:30809-75-7.mol

Synonyms:30809-75-7;4'-((4-Chlorophenyl)sulfonyl)-[1,1'-biphenyl]-4-ol;[1,1'-Biphenyl]-4-ol, 4'-[(4-chlorophenyl)sulfonyl]-;4-[4-(4-chlorophenyl)sulfonylphenyl]phenol;C18H13ClO3S;SCHEMBL720002;DTXSID00440169;MFCD30543160;DS-19654;CS-0163442;C74587;4'-(4-Chlorophenylsulfonyl)-1,1'-biphenyl-4-ol;A919551

Suppliers and Price of [1,1'-Biphenyl]-4-ol, 4'-[(4-chlorophenyl)sulfonyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of [1,1'-Biphenyl]-4-ol, 4'-[(4-chlorophenyl)sulfonyl]-

Chemical Property:

XLogP3:4.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:344.0273931
Heavy Atom Count:23
Complexity:463

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1C2=CC=C(C=C2)S(=O)(=O)C3=CC=C(C=C3)Cl)O

Technology Process of [1,1'-Biphenyl]-4-ol, 4'-[(4-chlorophenyl)sulfonyl]-

There total 4 articles about [1,1'-Biphenyl]-4-ol, 4'-[(4-chlorophenyl)sulfonyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 139225-66-4
4'-<(4-Chlorophenyl)sulfonyl>-3,5-di-tert-butyl-<1,1'-biphenyl>-4-ol

: 30809-75-7
4'-<(4-Chlorophenyl)sulfonyl>biphenyl-4-ol

Guidance literature:: With trifluorormethanesulfonic acid; toluene; at 100 ℃; for 3h;
DOI:10.1021/jo00095a024

Reference yield:

: 80-07-9,30605-10-8,85228-26-8,36313-66-3
4,4'-dichlorodiphenyl sulphone

: 71597-85-8
(p-hydroxyphenyl)boronic acid

: 30809-75-7
4'-<(4-Chlorophenyl)sulfonyl>biphenyl-4-ol

Guidance literature:: With sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; water; at 90 ℃; for 10h;

Reference yield:

: 80-07-9,30605-10-8,85228-26-8,36313-66-3
4,4'-dichlorodiphenyl sulphone

: 30809-75-7
4'-<(4-Chlorophenyl)sulfonyl>biphenyl-4-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / potassium tert-butoxide, quinoxaline / liquid ammonia / -38 °C / electrosynthesis: cathode - platinum grid, 10 cm², 1024 mesh/cm²; anode - magnesium rod, h = 8 cm, Φ = 1 cm; constant current density 0,5 A dm², KBr as supporting electrolyte

2: 80 percent / toluene, CF₃SO₃H / 3 h / 100 °C

With 2,3-diethynylquinoxaline; trifluorormethanesulfonic acid; potassium tert-butylate; toluene; In ammonia;
DOI:10.1021/jo00095a024