4-Nitrosobenzonitrile

Base Information

• Chemical Name: 4-Nitrosobenzonitrile
• CAS No.: 31125-07-2
• Molecular Formula: C7H4N2O
• Molecular Weight: 132.122
• Hs Code.: 2926909090
• Mol file: 31125-07-2.mol

Synonyms:4-cyano-nitrosobenzene;p-nitrosobenzonitrile;4-nitrosobenzonitrile;4-Nitroso-benzonitril;

Chemical Property of 4-Nitrosobenzonitrile

Chemical Property:

• PSA: 53.22000
• LogP: 1.95618

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Nitrosobenzonitrile

There total 11 articles about 4-Nitrosobenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

N-(4-cyanophenyl)hydroxylamine (24171-84-4) → 4-cyanonitrosobenzene (31125-07-2)

Guidance literature:

With tert-butylhypochlorite; In diethyl ether; at -78 - -20 ℃;

DOI:10.1021/jo990235x

Reference yield: 95.0%

4-Aminobenzonitrile (873-74-5) → 4-cyanonitrosobenzene (31125-07-2)

Guidance literature:

With oxone; In dichloromethane; water; at 20 ℃; for 1.5h;

DOI:10.1016/j.tetlet.2008.04.086

Reference yield: 37.0%

4-nitrobenzonitrile (619-72-7) → 4-cyanonitrosobenzene (31125-07-2)

Guidance literature:

With ammonium chloride; zinc; In ethanol; water; for 3h; Heating;

DOI:10.1016/0022-328X(89)80121-4

upstream raw materials:

4-Aminobenzonitrile

4-nitrobenzonitrile

N-(4-cyanophenyl)hydroxylamine

N-(4-cyanophenyl)acetohydroxamic acid

Downstream raw materials:

4,4'-(diazene-1,2-diyl)dibenzonitrile

4,4'-dicyanoazoxybenzene

4-cyano-N-methanesulphonylhydroxylamine

1,2-bis(4-cyanophenyl)diazene oxide

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