(3-BroMophenyl)(2-thienyl)Methanone

Base Information

• Chemical Name: (3-BroMophenyl)(2-thienyl)Methanone
• CAS No.: 31161-47-4
• Molecular Formula: C11H7BrOS
• Molecular Weight: 267.146
• Hs Code.: 2934999090
• Mol file: 31161-47-4.mol

Synonyms:(3-Bromophenyl)(2-thienyl)methanone;(3-Bromophenyl)(thiophen-2-yl)methanone;

Chemical Property of (3-BroMophenyl)(2-thienyl)Methanone

Chemical Property:

• PSA: 45.31000
• LogP: 3.74160

Purity/Quality:

97% ^*data from raw suppliers

(3-Bromophenyl)(2-thienyl)methanone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (3-BroMophenyl)(2-thienyl)Methanone

There total 3 articles about (3-BroMophenyl)(2-thienyl)Methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

thiophene (188290-36-0,8014-23-1,25233-34-5) + 3-bromobenzoyl chloride (1711-09-7) → (3-bromophenyl)(thiophen-2-yl)methanone (31161-47-4)

Guidance literature:

With aluminum (III) chloride; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere; Schlenk technique;

DOI:10.1002/ejoc.201403297

Reference yield:

m-bromobenzoic acid (585-76-2) → (3-bromophenyl)(thiophen-2-yl)methanone (31161-47-4)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride

2: 53 percent / AlCl₃ / Heating

With aluminium trichloride; thionyl chloride; 2: Friedels-Crafts benzoylation;

DOI:10.1002/jhet.5570400504

Reference yield:

→ (3-bromophenyl)(thiophen-2-yl)methanone (31161-47-4)

Guidance literature:

Thiophen, m-Brombenzoylchlorid/AlCl3;

upstream raw materials:

thiophene

3-bromobenzoyl chloride

m-bromobenzoic acid

Downstream raw materials:

2-Benzoylthiophene

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