1H-Indole-1-carboxylic acid, 2,3-dihydro-5-[(5R)-5-(hydroxymethyl)-2-oxo-3-oxazolidinyl]-2-methyl-, phenylmethyl ester, (2R)-

Base Information

Chemical Name:1H-Indole-1-carboxylic acid, 2,3-dihydro-5-[(5R)-5-(hydroxymethyl)-2-oxo-3-oxazolidinyl]-2-methyl-, phenylmethyl ester, (2R)-
CAS No.:312305-94-5
Molecular Formula:C₂₁H₂₂N₂O₅
Molecular Weight:382.416
Hs Code.:
Mol file:312305-94-5.mol

Synonyms:

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Chemical Property of 1H-Indole-1-carboxylic acid, 2,3-dihydro-5-[(5R)-5-(hydroxymethyl)-2-oxo-3-oxazolidinyl]-2-methyl-, phenylmethyl ester, (2R)-

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Technology Process of 1H-Indole-1-carboxylic acid, 2,3-dihydro-5-[(5R)-5-(hydroxymethyl)-2-oxo-3-oxazolidinyl]-2-methyl-, phenylmethyl ester, (2R)-

There total 5 articles about 1H-Indole-1-carboxylic acid, 2,3-dihydro-5-[(5R)-5-(hydroxymethyl)-2-oxo-3-oxazolidinyl]-2-methyl-, phenylmethyl ester, (2R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115210-54-3
2-methyl-5-nitroindoline

: 312305-94-5
benzyl (2R)-5-[(5R)-5-(hydroxymethyl)-2-oxo-1,3-oxazolidin-3-yl]-2-methyl-2,3-dihydro-1H-indole-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd/C / methanol

2: NaHCO₃ / acetone

3: n-BuLi / tetrahydrofuran

With n-butyllithium; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In tetrahydrofuran; methanol; acetone;
DOI:10.1016/j.bmcl.2003.07.029

Reference yield:

: 7570-47-0
5-nitro-2-methylindole

: 312305-94-5
benzyl (2R)-5-[(5R)-5-(hydroxymethyl)-2-oxo-1,3-oxazolidin-3-yl]-2-methyl-2,3-dihydro-1H-indole-1-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₃CN

2: H₂ / Pd/C / methanol

3: NaHCO₃ / acetone

4: n-BuLi / tetrahydrofuran

With n-butyllithium; hydrogen; sodium cyanoborohydride; sodium hydrogencarbonate; palladium on activated charcoal; In tetrahydrofuran; methanol; acetone;
DOI:10.1016/j.bmcl.2003.07.029

Reference yield:

: 103796-38-9
2-methyl-indolin-5-ylamine

: 312305-94-5
benzyl (2R)-5-[(5R)-5-(hydroxymethyl)-2-oxo-1,3-oxazolidin-3-yl]-2-methyl-2,3-dihydro-1H-indole-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: NaHCO₃ / acetone

2: n-BuLi / tetrahydrofuran

With n-butyllithium; sodium hydrogencarbonate; In tetrahydrofuran; acetone;
DOI:10.1016/j.bmcl.2003.07.029