4-BroMo-5-Methyl-3-phenylisoxazole

Base Information

Chemical Name:4-BroMo-5-Methyl-3-phenylisoxazole
CAS No.:31295-65-5
Molecular Formula:C10H8BrNO
Molecular Weight:238.084
Hs Code.:2934999090
Mol file:31295-65-5.mol

Synonyms:4-bromo-5-methyl-3-phenyl-isoxazole;4-Brom-5-methyl-3-phenyl-isoxazol;2-Phenyl-3-brom-4-methylisoxazol;3-Phenyl-4-brom-5-methylisoxazol;Isoxazole,4-bromo-5-methyl-3-phenyl;

Suppliers and Price of 4-BroMo-5-Methyl-3-phenylisoxazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
4-Bromo-5-methyl-3-phenylisoxazole 95+%
1g
$ 762.00

Chemenu
4-bromo-5-methyl-3-phenylisoxazole 95%
1g
$ 720.00

AK Scientific
4-Bromo-5-methyl-3-phenylisoxazole
2.5g
$ 1949.00

Total 8 raw suppliers

Chemical Property of 4-BroMo-5-Methyl-3-phenylisoxazole

Chemical Property:

Boiling Point:319.6±37.0 °C(Predicted)
PKA:-4.18±0.50(Predicted)
PSA：26.03000
Density:1.458±0.06 g/cm3(Predicted)
LogP:3.41250
Storage Temp.:2-8°C

Purity/Quality:

97% ^*data from raw suppliers

4-Bromo-5-methyl-3-phenylisoxazole 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-BroMo-5-Methyl-3-phenylisoxazole

There total 7 articles about 4-BroMo-5-Methyl-3-phenylisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1008-74-8
5-methyl-3-phenylisoxazole

: 31295-65-5
4-bromo-5-methyl-3-phenylisoxazole

Guidance literature:: With N-Bromosuccinimide; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1021/ol502246t

Reference yield:

: 68843-67-4
1-phenyl-but-3-en-1-one oxime

: 31295-65-5
4-bromo-5-methyl-3-phenylisoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; silver carbonate / chlorobenzene / 3 h / 70 °C

2: N-Bromosuccinimide / N,N-dimethyl-formamide / 2 h / 20 °C

With N-Bromosuccinimide; palladium diacetate; silver carbonate; In N,N-dimethyl-formamide; chlorobenzene;
DOI:10.1021/ol502246t

Reference yield:

: 80735-94-0,936-58-3
1-Phenyl-3-buten-1-ol

: 31295-65-5
4-bromo-5-methyl-3-phenylisoxazole

Guidance literature:: Multi-step reaction with 4 steps

1: Jones reagent / diethyl ether / 1 h / 0 - 20 °C

2: hydroxylamine hydrochloride; sodium acetate / water; ethanol / 20 °C

3: palladium diacetate; silver carbonate / chlorobenzene / 3 h / 70 °C

4: N-Bromosuccinimide / N,N-dimethyl-formamide / 2 h / 20 °C

With N-Bromosuccinimide; Jones reagent; hydroxylamine hydrochloride; sodium acetate; palladium diacetate; silver carbonate; In diethyl ether; ethanol; water; N,N-dimethyl-formamide; chlorobenzene;
DOI:10.1021/ol502246t