2,3,2',3'-tetra-O-acetyl-1,6-anhydro-4'-<2,4-di-O-acetyl-3,6-dideoxy-3-<(1S)-(1,4,6/5)-4,5,6-triacetoxy-3-acetoxymethyl-2-cyclohexenylamino>-α-D-gulopyranosyl>-β-maltose

Base Information

Chemical Name:2,3,2',3'-tetra-O-acetyl-1,6-anhydro-4'-<2,4-di-O-acetyl-3,6-dideoxy-3-<(1S)-(1,4,6/5)-4,5,6-triacetoxy-3-acetoxymethyl-2-cyclohexenylamino>-α-D-gulopyranosyl>-β-maltose
CAS No.:117011-94-6
Molecular Formula:C₄₇H₆₃NO₂₈
Molecular Weight:1090.01
Hs Code.:

2,3,2',3'-tetra-O-acetyl-1,6-anhydro-4'-<2,4-di-O-acetyl-3,6-dideoxy-3-<(1S)-(1,4,6/5)-4,5,6-triacetoxy-3-acetoxymethyl-2-cyclohexenylamino>-α-D-gulopyranosyl>-β-maltose

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Chemical Property of 2,3,2',3'-tetra-O-acetyl-1,6-anhydro-4'-<2,4-di-O-acetyl-3,6-dideoxy-3-<(1S)-(1,4,6/5)-4,5,6-triacetoxy-3-acetoxymethyl-2-cyclohexenylamino>-α-D-gulopyranosyl>-β-maltose

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Technology Process of 2,3,2',3'-tetra-O-acetyl-1,6-anhydro-4'-<2,4-di-O-acetyl-3,6-dideoxy-3-<(1S)-(1,4,6/5)-4,5,6-triacetoxy-3-acetoxymethyl-2-cyclohexenylamino>-α-D-gulopyranosyl>-β-maltose

There total 2 articles about 2,3,2',3'-tetra-O-acetyl-1,6-anhydro-4'-<2,4-di-O-acetyl-3,6-dideoxy-3-<(1S)-(1,4,6/5)-4,5,6-triacetoxy-3-acetoxymethyl-2-cyclohexenylamino>-α-D-gulopyranosyl>-β-maltose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90025-02-8
(1S,2S,3S,4R)-1-amino-5-(hydroxymethyl)-2,3:4,6-di-O-isopropylidene-5-cyclohexene-2,3,4-triol

: 117011-88-8
1,6-anhydro-4'-O-(3,4-anhydro-6-deoxy-α-D-galactopyranosyl)-β-maltose

: 117011-94-6
2,3,2',3'-tetra-O-acetyl-1,6-anhydro-4'-<2,4-di-O-acetyl-3,6-dideoxy-3-<(1S)-(1,4,6/5)-4,5,6-triacetoxy-3-acetoxymethyl-2-cyclohexenylamino>-α-D-gulopyranosyl>-β-maltose

: 117011-93-5
2,3,2',3',6',2'',3''-hepta-O-acetyl-1,6-anhydro-4'',6''-dideoxy-4''-<(1S)-(1,4,6/5)-4,5,6-triacetoxy-3-acetoxymethyl-2-cyclohexenylamino>-β-maltotriose

Guidance literature:: With acetic acid; Yield given. Multistep reaction. Yields of byproduct given; 1.) propan-2-ol, DMF, 120 deg C, 70 h, 3.) acetylation;
DOI:10.1039/c39880000605

Reference yield:

: 108-24-7
acetic anhydride

: 90025-02-8
(1S,2S,3S,4R)-1-amino-5-(hydroxymethyl)-2,3:4,6-di-O-isopropylidene-5-cyclohexene-2,3,4-triol

: 117011-88-8
1,6-anhydro-4'-O-(3,4-anhydro-6-deoxy-α-D-galactopyranosyl)-β-maltose

: 117011-94-6
2,3,2',3'-tetra-O-acetyl-1,6-anhydro-4'-<2,4-di-O-acetyl-3,6-dideoxy-3-<(1S)-(1,4,6/5)-4,5,6-triacetoxy-3-acetoxymethyl-2-cyclohexenylamino>-α-D-gulopyranosyl>-β-maltose

: 117011-93-5
2,3,2',3',6',2'',3''-hepta-O-acetyl-1,6-anhydro-4'',6''-dideoxy-4''-<(1S)-(1,4,6/5)-4,5,6-triacetoxy-3-acetoxymethyl-2-cyclohexenylamino>-β-maltotriose

Guidance literature:: Yield given. Multistep reaction. Yields of byproduct given; 1.) 2-propanol, N,N-dimethylformamide, sealed tube, 70 h, 120 deg C; 2.) aq. 70percent acetic acid, 2 h, 55 deg C; 3.) acetylation;
DOI:10.1016/0008-6215(89)84107-2