(6aR,9aR,11aR)-4-methyl-9-<2-(3'-O-tosyl-1',2'-O-isopropylidene-α-D-xylopentafuranoso)acetoxymethyl>-1,2,6a,7,10,10a-hexahydrothieno<3,2-a>anthracene-3,3,6,11-tetraone

Base Information

• Chemical Name: (6aR,9aR,11aR)-4-methyl-9-<2-(3'-O-tosyl-1',2'-O-isopropylidene-α-D-xylopentafuranoso)acetoxymethyl>-1,2,6a,7,10,10a-hexahydrothieno<3,2-a>anthracene-3,3,6,11-tetraone
• CAS No.: 130439-84-8
• Molecular Formula: C₃₄H₃₆O₁₂S₂
• Molecular Weight: 700.785

Synonyms:

Chemical Property of (6aR,9aR,11aR)-4-methyl-9-<2-(3'-O-tosyl-1',2'-O-isopropylidene-α-D-xylopentafuranoso)acetoxymethyl>-1,2,6a,7,10,10a-hexahydrothieno<3,2-a>anthracene-3,3,6,11-tetraone

Chemical Property:

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Technology Process of (6aR,9aR,11aR)-4-methyl-9-<2-(3'-O-tosyl-1',2'-O-isopropylidene-α-D-xylopentafuranoso)acetoxymethyl>-1,2,6a,7,10,10a-hexahydrothieno<3,2-a>anthracene-3,3,6,11-tetraone

There total 2 articles about (6aR,9aR,11aR)-4-methyl-9-<2-(3'-O-tosyl-1',2'-O-isopropylidene-α-D-xylopentafuranoso)acetoxymethyl>-1,2,6a,7,10,10a-hexahydrothieno<3,2-a>anthracene-3,3,6,11-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methyl-3,3-dioxi-1,2-dihydrothieno<3,2-a>naphthoquinone (130439-83-7) + 2-<2-(3'-O-tosyl-1',2'-O-isopropylidene-α-D-xylopentafuranoso)acetoxymethyl>-1,3-butadiene (303186-60-9) → (6aR,9aS,11aR)-4-methyl-9-<2-(3'-O-tosyl-1',2'-O-isopropylidene-α-D-xylopentafuranoso)acetoxymethyl>-1,2,6a,7,10,10a-hexahydrothieno<3,2-a>anthracene-3,3,6,11-tetraone (130548-63-9) + (6aR,9aR,11aR)-4-methyl-9-<2-(3'-O-tosyl-1',2'-O-isopropylidene-α-D-xylopentafuranoso)acetoxymethyl>-1,2,6a,7,10,10a-hexahydrothieno<3,2-a>anthracene-3,3,6,11-tetraone (130439-84-8) + acetic acid [2,2-dimethyl-6-(toluene-4-sulfonyloxy)-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl]-(4-methyl-3,3,6,11-tetraoxo-2,3,6,11-tetrahydro-1H-3λ6-anthra[2,1-b]thiophen-9-yl)-methyl ester (303186-67-6) + acetic acid [2,2-dimethyl-6-(toluene-4-sulfonyloxy)-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl]-(4-methyl-3,3,6,11-tetraoxo-2,3,6,11-tetrahydro-1H-3λ6-anthra[2,1-b]thiophen-9-yl)-methyl ester

Guidance literature:

In 1,4-dioxane; water; Heating;

Reference yield:

4-methyl-3,3-dioxi-1,2-dihydrothieno<3,2-a>naphthoquinone (130439-83-7) + 2-<2-(3'-O-tosyl-1',2'-O-isopropylidene-α-D-xylopentafuranoso)acetoxymethyl>-1,3-butadiene (303186-60-9) → (6aR,9aS,11aR)-4-methyl-9-<2-(3'-O-tosyl-1',2'-O-isopropylidene-α-D-xylopentafuranoso)acetoxymethyl>-1,2,6a,7,10,10a-hexahydrothieno<3,2-a>anthracene-3,3,6,11-tetraone (130548-63-9) + (6aR,9aR,11aR)-4-methyl-9-<2-(3'-O-tosyl-1',2'-O-isopropylidene-α-D-xylopentafuranoso)acetoxymethyl>-1,2,6a,7,10,10a-hexahydrothieno<3,2-a>anthracene-3,3,6,11-tetraone (130439-84-8)

Guidance literature:

Yield given. Yields of byproduct given;

upstream raw materials:

4-methyl-3,3-dioxi-1,2-dihydrothieno<3,2-a>naphthoquinone

2-<2-(3'-O-tosyl-1',2'-O-isopropylidene-α-D-xylopentafuranoso)acetoxymethyl>-1,3-butadiene

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