{manganese(II)(triphenylphosphine oxide)(NCS)2}

Base Information

• Chemical Name: {manganese(II)(triphenylphosphine oxide)(NCS)2}
• CAS No.: 129089-95-8
• Molecular Formula: C₂₀H₁₅MnN₂OPS₂
• Molecular Weight: 449.396
• Mol file: 129089-95-8.mol

Synonyms:

Chemical Property of {manganese(II)(triphenylphosphine oxide)(NCS)2}

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of {manganese(II)(triphenylphosphine oxide)(NCS)2}

There total 1 articles about {manganese(II)(triphenylphosphine oxide)(NCS)2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

manganese(II) thiocyanate (25327-03-1) + Triphenylphosphine oxide (791-28-6) → {manganese(II)(triphenylphosphine oxide)3(NCS)2} + di-μ-thiocyanato-bis{isothiocyanatobis(triphenylphosphine oxide)manganese(II)} + bis(isothiocyanato)tetrakis(triphenylphosphine oxide)manganese(II) + {manganese(II)(triphenylphosphine oxide)(NCS)2} (129089-95-8)

Guidance literature:

In toluene; addn. of OPPh3 to dried Mn(NCS)2 against a stream of Ar, then addn. of toluene, also against a stream of Ar, stirring the resulted slurry at room temp. for 7 h; isolation by standard Schlenk techniques, drying in vacuo, elem. anal.;

DOI:10.1039/DT9900001243

upstream raw materials:

manganese(II) thiocyanate

Triphenylphosphine oxide