N,N,N-Triethylethanaminium benzenethiolate

Base Information

Chemical Name:N,N,N-Triethylethanaminium benzenethiolate
CAS No.:3193-72-4
Molecular Formula:C8H20N.C6H5S
Molecular Weight:239.425
Hs Code.:
DSSTox Substance ID:DTXSID20579324
Mol file:3193-72-4.mol

Synonyms:3193-72-4;N,N,N-Triethylethanaminium benzenethiolate;tetraethylammonium thiophenolate;DTXSID20579324

Suppliers and Price of N,N,N-Triethylethanaminium benzenethiolate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of N,N,N-Triethylethanaminium benzenethiolate

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:239.17077098
Heavy Atom Count:16
Complexity:93.6

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC[N+](CC)(CC)CC.C1=CC=C(C=C1)[S-]

Technology Process of N,N,N-Triethylethanaminium benzenethiolate

There total 1 articles about N,N,N-Triethylethanaminium benzenethiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 77-98-5
tetraethylammonium hydroxide

: 108-98-5
thiophenol

: 3193-72-4
tetraethylammonium phenylthiolate

Guidance literature:: In methanol; at 20 ℃; for 0.5h;
DOI:10.1021/acs.joc.8b00143

Reference yield: 95.1%

: 14040-11-0
tungsten hexacarbonyl

: 3193-72-4
tetraethylammonium phenylthiolate

: 116148-13-1
{(C₂H₅)4N}⁽¹⁺⁾*{W(CO)5(S(C₆H₅))}^(1-) = {(C₂H₅)4N}{W(CO)5(S(C₆H₅))}

Guidance literature:: With THF; In tetrahydrofuran; Irradiation (UV/VIS); N2 atmosphere; addn. of soln. of W(CO)5*THF in THF (prepd. form photolysis of W(CO)6 in THF) to org. compd., stirring (15 min); pptn. on addn. of hexane, recrystn. (THF/hexane);

Reference yield: 94.2%

: 3193-72-4
tetraethylammonium phenylthiolate

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 116148-75-5
{(C₂H₅)4N}⁽¹⁺⁾*{Mo(CO)5(S(C₆H₅))}^(1-) = {(C₂H₅)4N}{Mo(CO)5(S(C₆H₅))}

Guidance literature:: In tetrahydrofuran; N2 atmosphere; addn. of Mo(CO)6 to org. compd. (N2 stream), addn. of THF, stirring (48 h); filt., washing ppt. with THF, combining soln., pptn. on concn. and addn. of hexane, recrystn. (THF/ diethyl ether/ hexane); IR monitoring;