(5S,6S)-6-[(E)-3-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-propenyl]-9-[1-butylsulfanyl-meth-(E)-ylidene]-4-methoxy-1-oxa-spiro[4.5]dec-3-ene-2,8-dione

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Chemical Name:(5S,6S)-6-[(E)-3-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-propenyl]-9-[1-butylsulfanyl-meth-(E)-ylidene]-4-methoxy-1-oxa-spiro[4.5]dec-3-ene-2,8-dione
CAS No.:123719-31-3
Molecular Formula:C₃₅H₄₄O₅SSi
Molecular Weight:604.883
Hs Code.:

(5S,6S)-6-[(E)-3-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-propenyl]-9-[1-butylsulfanyl-meth-(E)-ylidene]-4-methoxy-1-oxa-spiro[4.5]dec-3-ene-2,8-dione

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Chemical Property of (5S,6S)-6-[(E)-3-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-propenyl]-9-[1-butylsulfanyl-meth-(E)-ylidene]-4-methoxy-1-oxa-spiro[4.5]dec-3-ene-2,8-dione

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Technology Process of (5S,6S)-6-[(E)-3-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-propenyl]-9-[1-butylsulfanyl-meth-(E)-ylidene]-4-methoxy-1-oxa-spiro[4.5]dec-3-ene-2,8-dione

There total 1 articles about (5S,6S)-6-[(E)-3-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-propenyl]-9-[1-butylsulfanyl-meth-(E)-ylidene]-4-methoxy-1-oxa-spiro[4.5]dec-3-ene-2,8-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-79-5
n-butanethiol

: 123719-32-4
(5S,10S)-10-[(E)-3-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-propenyl]-4-methoxy-2-oxo-1-oxa-spiro[4.5]deca-3,7-diene-7-carbaldehyde

: 123719-31-3
(5S,6S)-6-[(E)-3-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-propenyl]-9-[1-butylsulfanyl-meth-(E)-ylidene]-4-methoxy-1-oxa-spiro[4.5]dec-3-ene-2,8-dione

Guidance literature:: With camphor-10-sulfonic acid; sodium methylate; magnesium sulfate; formic acid ethyl ester; Yield given. Multistep reaction; 1.) benzene; 2.) benzene, room temp.;
DOI:10.1039/c39890000221

Reference yield:

: 123719-31-3
(5S,6S)-6-[(E)-3-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-propenyl]-9-[1-butylsulfanyl-meth-(E)-ylidene]-4-methoxy-1-oxa-spiro[4.5]dec-3-ene-2,8-dione

: 123719-32-4
(5S,10S)-10-[(E)-3-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-propenyl]-4-methoxy-2-oxo-1-oxa-spiro[4.5]deca-3,7-diene-7-carbaldehyde

Guidance literature:: With hydrogenchloride; lithium triethylborohydride; mercury dichloride; Yield given. Multistep reaction; 1.) THF, -80 deg C, 15 min; 2.) acetone, room temp., 30 min;
DOI:10.1039/c39890000221

Reference yield:

: 123719-31-3
(5S,6S)-6-[(E)-3-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-propenyl]-9-[1-butylsulfanyl-meth-(E)-ylidene]-4-methoxy-1-oxa-spiro[4.5]dec-3-ene-2,8-dione

: Acetic acid (5S,10S)-10-[(E)-3-(tert-butyl-diphenyl-silanyloxy)-2-methyl-propenyl]-4-methoxy-2-oxo-1-oxa-spiro[4.5]deca-3,8-dien-(7E)-ylidenemethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) LiBEt₃H,; 2.) HgCl₂, HCl / 1.) THF, -80 deg C, 15 min; 2.) acetone, room temp., 30 min

2: 92 percent / Me₃SiCl, NaI / 0.67 h / 0-60 deg C

With hydrogenchloride; chloro-trimethyl-silane; lithium triethylborohydride; sodium iodide; mercury dichloride;
DOI:10.1039/c39890000221