Boc-Thr(CH2Ph)-Dopa(diCH2Ph)-Lys2(Cl)> p-nitrophenyl ester

Base Information

Chemical Name:Boc-Thr(CH2Ph)-Dopa(diCH2Ph)-Lys2(Cl)> p-nitrophenyl ester
CAS No.:111104-10-0
Molecular Formula:C₅₉H₆₄ClN₅O₁₃
Molecular Weight:1086.64
Hs Code.:

Boc-Thr(CH2Ph)-Dopa(diCH2Ph)-Lys<Z<sup>2</sup>(Cl)> p-nitrophenyl ester

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Chemical Property of Boc-Thr(CH2Ph)-Dopa(diCH2Ph)-Lys2(Cl)> p-nitrophenyl ester

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Technology Process of Boc-Thr(CH2Ph)-Dopa(diCH2Ph)-Lys2(Cl)> p-nitrophenyl ester

There total 5 articles about Boc-Thr(CH2Ph)-Dopa(diCH2Ph)-Lys2(Cl)> p-nitrophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59727-98-9
3-[3,4-di(benzyloxy)phenyl]-2-{[(tert-butoxy)carbonyl]amino}propanoic acid

: 111104-10-0
Boc-Thr(CH2Ph)-Dopa(diCH2Ph)-Lys2(Cl)> p-nitrophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) N-methylmorpholine; 2.) DCCI / 2.) chloroform; 3.) chloroform, 0 deg C, 2 h, 5 deg C, overnight

2: 1.) 1.1 M HCl / 1.) dioxane, RT, 1 h; 2.) ether, dioxane, RT, 2 h, overnight, refrigerator

3: 1.) N-methylmorpholine; 2.) DCCI / 2.) chloroform; 3.) chloroform, 0 deg C, 2 h, 5 deg C, overnight

With 4-methyl-morpholine; hydrogenchloride; dicyclohexyl-carbodiimide;

Reference yield:

: 30033-24-0
(2S)-3-(3,4-dihydroxyphenyl)-2-[(tert-butoxy)carbonylamino]propanoic acid

: 111104-10-0
Boc-Thr(CH2Ph)-Dopa(diCH2Ph)-Lys2(Cl)> p-nitrophenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 51 percent / potassium carbonate, sodium iodide

2: 1.) N-methylmorpholine; 2.) DCCI / 2.) chloroform; 3.) chloroform, 0 deg C, 2 h, 5 deg C, overnight

3: 1.) 1.1 M HCl / 1.) dioxane, RT, 1 h; 2.) ether, dioxane, RT, 2 h, overnight, refrigerator

4: 1.) N-methylmorpholine; 2.) DCCI / 2.) chloroform; 3.) chloroform, 0 deg C, 2 h, 5 deg C, overnight

With 4-methyl-morpholine; hydrogenchloride; potassium carbonate; dicyclohexyl-carbodiimide; sodium iodide;

Reference yield:

: 100-44-7
benzyl chloride

: 111104-10-0
Boc-Thr(CH2Ph)-Dopa(diCH2Ph)-Lys2(Cl)> p-nitrophenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 51 percent / potassium carbonate, sodium iodide

2: 1.) N-methylmorpholine; 2.) DCCI / 2.) chloroform; 3.) chloroform, 0 deg C, 2 h, 5 deg C, overnight

3: 1.) 1.1 M HCl / 1.) dioxane, RT, 1 h; 2.) ether, dioxane, RT, 2 h, overnight, refrigerator

4: 1.) N-methylmorpholine; 2.) DCCI / 2.) chloroform; 3.) chloroform, 0 deg C, 2 h, 5 deg C, overnight

With 4-methyl-morpholine; hydrogenchloride; potassium carbonate; dicyclohexyl-carbodiimide; sodium iodide;