N-phenylcitraconamic acid tributylstannyl ester

Base Information

• Chemical Name: N-phenylcitraconamic acid tributylstannyl ester
• CAS No.: 133710-00-6
• Molecular Formula: C₂₃H₃₇NO₃Sn
• Molecular Weight: 494.262
• Mol file: 133710-00-6.mol

Synonyms:

Chemical Property of N-phenylcitraconamic acid tributylstannyl ester

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

Technology Process of N-phenylcitraconamic acid tributylstannyl ester

There total 1 articles about N-phenylcitraconamic acid tributylstannyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(Z)-2-methyl-4-oxo-4-(phenylamino)but-2-enoic acid (80818-21-9) + bis(tri-n-butyltin)oxide (56-35-9) → N-phenylcitraconamic acid tributylstannyl ester (133710-00-6)

Guidance literature:

In toluene; byproducts: H2O; refluxing a mixture of tin-compd. with amic acid (ratio 1:2) for 1-2 h, removal of H2O by azeotropic dehydration (Dean and Stark trap); recrystn. from light petroleum; elem. anal.;

DOI:10.1016/0022-328X(91)86246-M

upstream raw materials:

(Z)-2-methyl-4-oxo-4-(phenylamino)but-2-enoic acid

bis(tri-n-butyltin)oxide