[10-[2-[(2-methoxy-6-nitrophenyl)amino]-2-(oxo-κO)ethyl]-1,4,7,10-tetraazacyclododecane-1,4,7-triacetato(3-)-κN1,.kapp.N4,κN7,κN10,κO1,κO4,κO7]gadolinium

Base Information

Chemical Name:[10-[2-[(2-methoxy-6-nitrophenyl)amino]-2-(oxo-κO)ethyl]-1,4,7,10-tetraazacyclododecane-1,4,7-triacetato(3-)-κN1,.kapp.N4,κN7,κN10,κO1,κO4,κO7]gadolinium
CAS No.:1206903-27-6
Molecular Formula:C₂₃H₃₁GdN₆O₁₀
Molecular Weight:708.783
Hs Code.:

[10-[2-[(2-methoxy-6-nitrophenyl)amino]-2-(oxo-κO)ethyl]-1,4,7,10-tetraazacyclododecane-1,4,7-triacetato(3-)-κN1,.kapp.N4,κN7,κN10,κO1,κO4,κO7]gadolinium

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Chemical Property of [10-[2-[(2-methoxy-6-nitrophenyl)amino]-2-(oxo-κO)ethyl]-1,4,7,10-tetraazacyclododecane-1,4,7-triacetato(3-)-κN1,.kapp.N4,κN7,κN10,κO1,κO4,κO7]gadolinium

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Technology Process of [10-[2-[(2-methoxy-6-nitrophenyl)amino]-2-(oxo-κO)ethyl]-1,4,7,10-tetraazacyclododecane-1,4,7-triacetato(3-)-κN1,.kapp.N4,κN7,κN10,κO1,κO4,κO7]gadolinium

There total 1 articles about [10-[2-[(2-methoxy-6-nitrophenyl)amino]-2-(oxo-κO)ethyl]-1,4,7,10-tetraazacyclododecane-1,4,7-triacetato(3-)-κN1,.kapp.N4,κN7,κN10,κO1,κO4,κO7]gadolinium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1206903-33-4
10-[2-[(2-methoxy-6-nitrophenyl)amino]-2-oxoethyl]-1,4,7,10-tetraazacyclododecane-1,4,7-triacetic acid

: gadolinium(III) trifluoromethanesulfonate

: 1206903-27-6
[10-[2-[(2-methoxy-6-nitrophenyl)amino]-2-(oxo-κO)ethyl]-1,4,7,10-tetraazacyclododecane-1,4,7-triacetato(3-)-κN1,.kapp.N4,κN7,κN10,κO1,κO4,κO7]gadolinium

Guidance literature:: In methanol; mixt. Gd(OTf)3 and ligand was stirred in MeOH at 50°C for 24 h; mixt. was concd., added dropwise under stirring to Et2O at 0°C, ppt. was filtered, washed with Et2O, dried;
DOI:10.1002/hlca.200900108