Technology Process of 5,5-dicarbonyl-2,2-diethyl-5-(triphenylphosphine)-1λ3-thia-2λ5-phospha-5-cobalta-1,3-cyclopentadiene-3,4-carboxylic acid dicyclohexyl ester
There total 1 articles about 5,5-dicarbonyl-2,2-diethyl-5-(triphenylphosphine)-1λ3-thia-2λ5-phospha-5-cobalta-1,3-cyclopentadiene-3,4-carboxylic acid dicyclohexyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
toluene;
To Co(CO)2PPh3SPEt2 and PPh3 was added CyO2CCCCO2Cy dropwise at 55 °C. After 2 h the soln. was dried, CH3-Cy was added, filtered and dried, dissolved in EtOH/toluene, filtered. Soln. was dried, dissolved in toluene/EtOH for 24 h at -5 °C.; Crystn. at -30 °C, recrystn. from 15 ml toluene and 45 ml CH3-Cy at -5 °C after filtration, elem. anal.;
