5-(2-METHYL-4-NITROPHENYL)-2-FURALDEHYDE

Base Information

• Chemical Name: 5-(2-METHYL-4-NITROPHENYL)-2-FURALDEHYDE
• CAS No.: 329222-70-0
• Molecular Formula: C12H9NO4
• Molecular Weight: 231.208
• Hs Code.: 2932190090
• Mol file: 329222-70-0.mol

Synonyms:5-(2-Methyl-4-nitrophenyl)-2-furaldehyde;2-Furancarboxaldehyde,5-(2-methyl-4-nitrophenyl);5-(2-Methyl-4-nitro-phenyl)-furan-2-carbaldehyde;TOS-BB-0640;

Chemical Property of 5-(2-METHYL-4-NITROPHENYL)-2-FURALDEHYDE

Chemical Property:

• Vapor Pressure: 1.4E-06mmHg at 25°C
• Boiling Point: 399.1oC at 760 mmHg
• Flash Point: 195.2oC
• PSA: 76.03000
• Density: 1.304g/cm3
• LogP: 3.49890

Purity/Quality:

97% ^*data from raw suppliers

5-(2-Methyl-4-nitrophenyl)-2-furaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-(2-METHYL-4-NITROPHENYL)-2-FURALDEHYDE

There total 1 articles about 5-(2-METHYL-4-NITROPHENYL)-2-FURALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

furfural (98-01-1) + 5-nitro-toluene-2-diazonium ; chloride (69457-09-6) → 5-(2-methyl-4-nitrophenyl)furan-2-carbaldehyde (329222-70-0)

Guidance literature:

With copper(l) chloride; In water; at 20 ℃; for 48h;

DOI:10.1016/S0957-4166(03)00286-6

Reference yield: 88.0%

vinyl n-butyrate (123-20-6,24991-31-9) + 2-hydroxy-2-methylpropanenitrile (75-86-5) + 5-(2-methyl-4-nitrophenyl)furan-2-carbaldehyde (329222-70-0) → (R)-[5-(2-methyl-4-nitrophenyl)furan-2-yl]cyanomethyl butanoate

Guidance literature:

With Pseudomonas cepacia lipase; Amberlite IRA 904 (OH(-) form); In toluene; at 22 - 23 ℃; for 168h;

DOI:10.1016/S0957-4166(03)00286-6

Reference yield: 83.0%

4-(4-chloro-phenyl)-6-(2,4-dichloro-5-fluoro-phenyl)-3,4-dihydro-1H-pyrimidine-2-thione (777859-11-7) + chloroacetic acid (79-11-8) + 5-(2-methyl-4-nitrophenyl)furan-2-carbaldehyde (329222-70-0) → 5-(4-chloro-phenyl)-7-(2,4-dichloro-5-fluoro-phenyl)-2-[5-(2-methyl-4-nitro-phenyl)-furan-2-ylmethylene]-5H-thiazolo[3,2-a]pyrimidin-3-one

Guidance literature:

With sodium acetate; In acetic anhydride; acetic acid; for 3h; Heating;

DOI:10.1016/j.ejmech.2004.06.001

upstream raw materials:

furfural

5-nitro-toluene-2-diazonium ; chloride

Downstream raw materials:

hydroxy-[5-(2-methyl-4-nitrophenyl)-furan-2-yl]acetonitrile

[5-(2-methyl-4-nitrophenyl)furan-2-yl]cyanomethyl butanoate

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