methyl 3,3-dimethylbicyclo[2.2.1]hept-5-ene-2-carboxylate

Base Information

• Chemical Name: methyl 3,3-dimethylbicyclo[2.2.1]hept-5-ene-2-carboxylate
• CAS No.: 83846-54-2
• Molecular Formula: C11H16 O2
• Molecular Weight: 180.247
• Hs Code.: 2916209090
• Mol file: 83846-54-2.mol

Synonyms:5-Norbornene-2-carboxylicacid, 3,3-dimethyl-, methyl ester (6CI)

Chemical Property of methyl 3,3-dimethylbicyclo[2.2.1]hept-5-ene-2-carboxylate

Chemical Property:

• Vapor Pressure: 0.146mmHg at 25°C
• Boiling Point: 215.6°C at 760 mmHg
• Flash Point: 75°C
• PSA: 26.30000
• Density: 1.032g/cm³
• LogP: 2.00770

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of methyl 3,3-dimethylbicyclo[2.2.1]hept-5-ene-2-carboxylate

There total 3 articles about methyl 3,3-dimethylbicyclo[2.2.1]hept-5-ene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

Methyl 3,3-dimethylacrylate (924-50-5) + cyclopenta-1,3-diene (542-92-7,25568-84-7,7313-32-8) → 5-carbomethoxy-6,6-dimethyl-2-norbornene (83846-54-2)

Guidance literature:

at 140 ℃; for 504h; sealed tube;

DOI:10.1021/ja00265a029

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) → (+/-)-3,3-dimethyl-norborn-5-ene-2exo-carboxylic acid methyl ester (81216-25-3,81216-27-5,83846-54-2)

Guidance literature:

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) → (+/-)-3,3-dimethyl-norborn-5-ene-2endo-carboxylic acid methyl ester (81216-25-3,81216-27-5,83846-54-2)

Guidance literature:

upstream raw materials:

diazomethane

Methyl 3,3-dimethylacrylate

cyclopenta-1,3-diene

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