3-(Tributylstannyl)pyridazine

Base Information

• Chemical Name: 3-(Tributylstannyl)pyridazine
• CAS No.: 332133-93-4
• Molecular Formula: C16H30N2Sn
• Molecular Weight: 369.138
• European Community (EC) Number: 815-738-6
• Mol file: 332133-93-4.mol

Synonyms:3-(TRIBUTYLSTANNYL)PYRIDAZINE;332133-93-4;tributyl(pyridazin-3-yl)stannane;3-TRIBUTYLSTANNANYL-PYRIDAZINE;Pyridazine, 3-(tributylstannyl)-;3-(tributylstannanyl)pyridazine;tributylstannylpyridazine;tri-n-butylstannylpyridazine;SCHEMBL304795;DBHSVKZZSWTSTN-UHFFFAOYSA-N;MFCD07787370;AKOS027324769;AB42962;A50081;A902317

Chemical Property of 3-(Tributylstannyl)pyridazine

Chemical Property:

• Boiling Point: 406.9±37.0 °C(Predicted)
• PKA: 2.83±0.10(Predicted)
• PSA: 25.78000
• LogP: 4.22240
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 10
• Exact Mass: 370.143102
• Heavy Atom Count: 19
• Complexity: 199

Purity/Quality:

97% ^*data from raw suppliers

3-(Tributylstannyl)pyridazine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCC[Sn](CCCC)(CCCC)C1=NN=CC=C1

Technology Process of 3-(Tributylstannyl)pyridazine

There total 1 articles about 3-(Tributylstannyl)pyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ tributyl(pyridazin-3-yl)stannane (332133-93-4)

Guidance literature:

Reference yield: 43.0%

1-[(tert-butyldimethylsilyl)oxy]-1-(5-iodooxazol-2-yl)-7-phenylheptane (808134-97-6) + tributyl(pyridazin-3-yl)stannane (332133-93-4) → 1-[(tert-butyldimethylsilyl)oxy]-1-[5-(3-pyridazinyl)oxazol-2-yl]-7-phenylheptane (808134-99-8)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; at 100 ℃;

DOI:10.1021/jm049614v

Reference yield: 8.0%

5-iodo-1-{3-[(1S,5R)-1-(4-trifluoromethyl-phenyl)-3-aza-bicyclo[3.1.0]hex-3-yl]-propyl}-1H-pyrimidine-2,4-dione (952402-39-0) + tributyl(pyridazin-3-yl)stannane (332133-93-4) → 5-(3-pyridazinyl)-1-(3-{(1S,5R)-1-[4-(trifluoromethyl)phenyl]-3-azabicyclo[3.1.0]hex-3-yl}propyl)-2,4(1H,3H)-pyrimidinedione (952401-80-8)

Guidance literature:

tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 90 ℃; for 4h; Product distribution / selectivity;

Downstream raw materials:

1-[(tert-butyldimethylsilyl)oxy]-1-[5-(3-pyridazinyl)oxazol-2-yl]-7-phenylheptane

5-(3-pyridazinyl)-1-(3-{(1S,5R)-1-[4-(trifluoromethyl)phenyl]-3-azabicyclo[3.1.0]hex-3-yl}propyl)-2,4(1H,3H)-pyrimidinedione

4-(3-methoxy-5-methyl-phenyl)-2-[5-(pyridazin-3-yl)-2-trifluoromethyl-phenyl]-2,5,6,7-tetrahydro-cyclopenta[d]pyridazin-1-one

di-tert-butyl {(4aR,6R,8aS)-8a-(2-fluoro-5-pyridazin-3-ylphenyl)-6-methoxymethyl-4,4a,5,6,8,8a-hexahydropyrano[3,4-d][1,3]thiazin-2-yl}imidodicarbonate

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