5-Chlorobenzo[b]phosphindole

Base Information

Chemical Name:5-Chlorobenzo[b]phosphindole
CAS No.:33300-85-5
Molecular Formula:C12H8ClP
Molecular Weight:218.622
Hs Code.:2934999090
Nikkaji Number:J876.092F
Mol file:33300-85-5.mol

Synonyms:5-chlorobenzo[b]phosphindole;5-CHLORO-5H-DIBENZOPHOSPHOLE;5-chlorodibenzophosphole;SCHEMBL7704265;ONQRFNKLTKSHEJ-UHFFFAOYSA-N

Suppliers and Price of 5-Chlorobenzo[b]phosphindole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
5-Chlorobenzo[b]phosphindole
1g
$ 349.00

Sigma-Aldrich
5-Chlorobenzo[b]phosphindole
250mg
$ 96.40

American Custom Chemicals Corporation
5-CHLORO-5H-DIBENZOPHOSPHOLE 95.00%
25G
$ 1395.88

Total 17 raw suppliers

Chemical Property of 5-Chlorobenzo[b]phosphindole

Chemical Property:

Melting Point:146-179°C
Boiling Point:146-148 °C(Press: 5 Torr)
PSA：0.00000
LogP:4.98150
XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:218.0052149
Heavy Atom Count:14
Complexity:196

Purity/Quality:

99% ^*data from raw suppliers

5-Chlorobenzo[b]phosphindole ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C3=CC=CC=C3P2Cl

Technology Process of 5-Chlorobenzo[b]phosphindole

There total 7 articles about 5-Chlorobenzo[b]phosphindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 16291-32-0
biphenyl-2,2'-diyl-bis-lithium

: 33300-85-5
9-Chlorodibenzophosphole

Guidance literature:: With phosphorus trichloride; In tetrahydrofuran;
DOI:10.1080/10426509608037969

Reference yield:

: 13029-09-9
2,2'-dibromobiphenyl

: 33300-85-5
9-Chlorodibenzophosphole

Guidance literature:: 2,2'-dibromobiphenyl; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; for 4h; Inert atmosphere;

With phosphorus trichloride; In tetrahydrofuran; pentane; at -198 - 20 ℃; Inert atmosphere;
DOI:10.1246/cl.2011.174

Reference yield:

: 13029-09-9
2,2'-dibromobiphenyl

: 5-bromo-5H-dibenzophosphole

: 33300-85-5
9-Chlorodibenzophosphole

Guidance literature:: 2,2'-dibromobiphenyl; With n-butyllithium; In diethyl ether; hexane; at 0 - 25 ℃; for 1h; Inert atmosphere; Schlenk technique;

With phosphorus trichloride; In diethyl ether; hexane; at -198 - 25 ℃; for 0.25h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c5dt02976g