3a,6-dihydro-2,4,6-triphenyl-1,3,3a,5-tetraazabenzazulene

Base Information

• Chemical Name: 3a,6-dihydro-2,4,6-triphenyl-1,3,3a,5-tetraazabenzazulene
• CAS No.: 91867-99-1
• Molecular Formula: C₂₂H₁₆N₄
• Molecular Weight: 336.396
• Mol file: 91867-99-1.mol

Synonyms:

Chemical Property of 3a,6-dihydro-2,4,6-triphenyl-1,3,3a,5-tetraazabenzazulene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3a,6-dihydro-2,4,6-triphenyl-1,3,3a,5-tetraazabenzazulene

There total 2 articles about 3a,6-dihydro-2,4,6-triphenyl-1,3,3a,5-tetraazabenzazulene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.3%

2,3,6,7-tetraphenyl<1,2,3>triazolo<2,1-a><1,2,3>triazole (91666-82-9) → 3a,6-dihydro-2,4,6-triphenyl-1,3,3a,5-tetraazabenzazulene (91867-99-1) + 1,2-diphenyl-1-(3,5-diphenyl-1H-1,2,4-triazol-1-yl)-2H-azirine (91666-85-2) + 1,2-diphenyl-1-(4,5-diphenyl-2H-1,2,3-triazol-2-yl)-2H-azirine (91666-83-0) + 2,3,5,7-tetraphenyl-1,2,3-triazolo<1,2-a>-1,2,4-triazole

Guidance literature:

In tetrahydrofuran; at 22 - 25 ℃; Irradiation; λ>270 nm;

DOI:10.1016/S0040-4039(01)81244-2

Reference yield:

→ 3a,6-dihydro-2,4,6-triphenyl-1,3,3a,5-tetraazabenzazulene (91867-99-1) + 1,2-diphenyl-1-(3,5-diphenyl-1H-1,2,4-triazol-1-yl)-2H-azirine (91666-85-2) + 1,2-diphenyl-1-(4,5-diphenyl-2H-1,2,3-triazol-2-yl)-2H-azirine (91666-83-0) + 2,3,5,7-tetraphenyl-1,2,3-triazolo<1,2-a>-1,2,4-triazole

Guidance literature:

In tetrahydrofuran; at 22 - 25 ℃; Irradiation; λ>270 nm;

DOI:10.1016/S0040-4039(01)81244-2

upstream raw materials:

2,3,6,7-tetraphenyl<1,2,3>triazolo<2,1-a><1,2,3>triazole