Acetamide, 2-chloro-N-(2,6-dimethyl-4-oxo-2,5-cyclohexadien-1-ylidene)-

Base Information

Chemical Name:Acetamide, 2-chloro-N-(2,6-dimethyl-4-oxo-2,5-cyclohexadien-1-ylidene)-
CAS No.:206439-03-4
Molecular Formula:C₁₀H₁₀ClNO₂
Molecular Weight:211.648
Hs Code.:
DSSTox Substance ID:DTXSID00174679
Nikkaji Number:J909.280C

Synonyms:2,6-Dimethylchloroacetylquinoneimine;Acetamide, 2-chloro-N-(2,6-dimethyl-4-oxo-2,5-cyclohexadien-1-ylidene)-;2-Chloro-N-(2,6-dimethyl-4-oxo-2,5-cyclohexadien-1-ylidene)acetamide;206439-03-4;DTXSID00174679;LS-8508;N-(Chloroacetyl)-3,5-dimethyl-p-benzoquinone imine

Suppliers and Price of Acetamide, 2-chloro-N-(2,6-dimethyl-4-oxo-2,5-cyclohexadien-1-ylidene)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Acetamide, 2-chloro-N-(2,6-dimethyl-4-oxo-2,5-cyclohexadien-1-ylidene)-

Chemical Property:

Vapor Pressure:0.000552mmHg at 25°C
Boiling Point:311.8°C at 760 mmHg
Flash Point:114.3°C
Density:1.23g/cm³
XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:211.0400063
Heavy Atom Count:14
Complexity:354

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=O)C=C(C1=NC(=O)CCl)C

Technology Process of Acetamide, 2-chloro-N-(2,6-dimethyl-4-oxo-2,5-cyclohexadien-1-ylidene)-

There total 4 articles about Acetamide, 2-chloro-N-(2,6-dimethyl-4-oxo-2,5-cyclohexadien-1-ylidene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 857570-22-0
N-Chloroacetyl-3,5-dimethyl-4-aminophenol

: 206439-03-4
N-Chloroacetyl-3,5-dimethyl-p-benzoquinone-4-imine

Guidance literature:: With palladium(II) acetate; In ethyl acetate; at 0 - 5 ℃; for 0.166667h;
DOI:10.1016/S1383-5718(97)00163-0

Reference yield:

: 3096-70-6
3,5-dimethyl-4-aminophenol

: 206439-03-4
N-Chloroacetyl-3,5-dimethyl-p-benzoquinone-4-imine

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / toluene; tetrahydrofuran / 0.17 h / 0 °C

2: Pd(OAc)4 / ethyl acetate / 0.17 h / 0 - 5 °C

With palladium(II) acetate; triethylamine; In tetrahydrofuran; ethyl acetate; toluene;
DOI:10.1016/S1383-5718(97)00163-0

Reference yield:

: 108-68-9,50356-23-5
3,5-Dimethylphenol

: 206439-03-4
N-Chloroacetyl-3,5-dimethyl-p-benzoquinone-4-imine

Guidance literature:: Multi-step reaction with 4 steps

2: Na₂S₂O₄ / 65 °C

3: Et₃N / toluene; tetrahydrofuran / 0.17 h / 0 °C

4: Pd(OAc)4 / ethyl acetate / 0.17 h / 0 - 5 °C

With palladium(II) acetate; sodium dithionite; triethylamine; In tetrahydrofuran; ethyl acetate; toluene;
DOI:10.1016/S1383-5718(97)00163-0