1H-Benzimidazole, 2-(2-naphthalenyl)-

Base Information

Chemical Name:1H-Benzimidazole, 2-(2-naphthalenyl)-
CAS No.:3367-02-0
Molecular Formula:C17H12N2
Molecular Weight:244.296
Hs Code.:2934999090
DSSTox Substance ID:DTXSID80402326
Nikkaji Number:J1.105.418H
Wikidata:Q82205723
Mol file:3367-02-0.mol

Synonyms:3367-02-0;1H-Benzimidazole, 2-(2-naphthalenyl)-;2-naphthalen-2-yl-1H-benzimidazole;2-(Naphthalen-2-yl)-1H-benzo[d]imidazole;2- Naphtyl-Benzimidazol;SCHEMBL784354;DTXSID80402326;2-(2-Naphthyl)-1H-benzimidazole;AKOS008956973;1h-benzo[d]imidazole,2-(2-naphthalenyl)-;FT-0743462

Suppliers and Price of 1H-Benzimidazole, 2-(2-naphthalenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 1H-Benzimidazole, 2-(2-naphthalenyl)-

Chemical Property:

Melting Point:260-262 °C(Solv: ethanol, 30% (64-17-5))
Boiling Point:490.5±28.0 °C(Predicted)
PKA:11.41±0.10(Predicted)
PSA：28.68000
Density:1.256±0.06 g/cm3(Predicted)
LogP:4.38310
XLogP3:4.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:244.100048391
Heavy Atom Count:19
Complexity:316

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C=C(C=CC2=C1)C3=NC4=CC=CC=C4N3

Technology Process of 1H-Benzimidazole, 2-(2-naphthalenyl)-

There total 3 articles about 1H-Benzimidazole, 2-(2-naphthalenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 3-(naphthalen-2-yl)-4,5-diphenyl-4,5-dihydro-1,2,4-oxadiazole

: 67-68-5,8070-53-9
dimethyl sulfoxide

: N-(dimethyl(oxo)-λ6-sulfanylidene)-N'-phenyl-2-naphthimidamide

: 3367-02-0
2-(naphthalen-2-yl)-1H-1,3-benzodiazole

Guidance literature:: With fac-tris(2-phenylpyridinato-N,C₂')iridium(III); at 20 - 22 ℃; Sealed tube; Irradiation; Inert atmosphere;
DOI:10.1021/acs.orglett.9b04646

Reference yield:

: 51873-98-4,57207-34-8,24091-02-9
2-naphthaldoxime

: N-(dimethyl(oxo)-λ6-sulfanylidene)-N'-phenyl-2-naphthimidamide

: 3367-02-0
2-(naphthalen-2-yl)-1H-1,3-benzodiazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide; dichloromethane / 20 - 22 °C

1.2: 0 - 22 °C

2.1: fac-tris(2-phenylpyridinato-N,C₂')iridium(III) / 20 - 22 °C / Sealed tube; Irradiation; Inert atmosphere

With N-chloro-succinimide; fac-tris(2-phenylpyridinato-N,C₂')iridium(III); In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/acs.orglett.9b04646

Reference yield:

: 538-51-2
benzylidene phenylamine

: N-(dimethyl(oxo)-λ6-sulfanylidene)-N'-phenyl-2-naphthimidamide

: 3367-02-0
2-(naphthalen-2-yl)-1H-1,3-benzodiazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide; dichloromethane / 20 - 22 °C

1.2: 0 - 22 °C

2.1: fac-tris(2-phenylpyridinato-N,C₂')iridium(III) / 20 - 22 °C / Sealed tube; Irradiation; Inert atmosphere

With N-chloro-succinimide; fac-tris(2-phenylpyridinato-N,C₂')iridium(III); In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/acs.orglett.9b04646