Dibenzylzink-1,4-dioxan

Base Information

• Chemical Name: Dibenzylzink-1,4-dioxan
• CAS No.: 76721-55-6
• Molecular Formula: C₁₈H₂₂O₂Zn
• Molecular Weight: 335.761
• Mol file: 76721-55-6.mol

Synonyms:

Chemical Property of Dibenzylzink-1,4-dioxan

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Dibenzylzink-1,4-dioxan

There total 1 articles about Dibenzylzink-1,4-dioxan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-dioxane (123-91-1,28347-88-8,28347-91-3,39449-24-6,54841-74-6) + zinc(II) chloride (7646-85-7,24359-56-6) + benzylmagnesium chloride (6921-34-2) → Dibenzylzink-1,4-dioxan (76721-55-6)

Guidance literature:

In diethyl ether; byproducts: MgCl2; the mixture of ZnCl2 and PhMgCl was refluxed for 3 h, 1,4-dioxane was added to the soln.; filtered, filtrate evapd. in vac., crystd. by adding n-hexane; elem anal.;

Reference yield:

Dibenzylzink-1,4-dioxan (76721-55-6) → dibenzylzinc (7029-30-3)

Guidance literature:

heated in 0.1 torr at 50-60°C for 10 h;

upstream raw materials:

1,4-dioxane

zinc(II) chloride

benzylmagnesium chloride

Downstream raw materials:

dibenzylzinc