ClCH₂Pb(C₆H₅)3

Base Information

• Chemical Name: ClCH₂Pb(C₆H₅)3
• CAS No.: 134152-41-3
• Molecular Formula: C₁₉H₁₇ClPb
• Molecular Weight: 487.997
• Mol file: 134152-41-3.mol

Synonyms:

Chemical Property of ClCH₂Pb(C₆H₅)3

Chemical Property:

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Technology Process of ClCH₂Pb(C₆H₅)3

There total 1 articles about ClCH₂Pb(C₆H₅)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

chlorobromomethane (74-97-5) + triphenyllead(IV) chloride (1153-06-6) → ClCH2Pb(C6H5)3 (134152-41-3)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; (N2) or (Ar), to ClPbPh3 and BrClCH2 in THF added n-butyllithium in hexane at -70°C, warmed to room temp. over 45 min; hydrolized, extracted with CH2Cl2, washed with H2O, dried over CaCl2, solvent removed, recrystd. from hot hexane, evapd., recrystd., elem. anal.;

DOI:10.1021/om00052a049

upstream raw materials:

chlorobromomethane

triphenyllead(IV) chloride