benzyl-methoxy-dimethylgermane

Base Information

Chemical Name:benzyl-methoxy-dimethylgermane
CAS No.:153771-89-2
Molecular Formula:C₁₀H₁₆GeO
Molecular Weight:224.826
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl-methoxy-dimethylgermane

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Technology Process of benzyl-methoxy-dimethylgermane

There total 1 articles about benzyl-methoxy-dimethylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 82546-74-5
benzoylchlorodimethylgermane

: 153771-89-2
benzyl-methoxy-dimethylgermane

Guidance literature:: With n-butyl lithium; methanol; In hexane; byproducts: LiCl; N2 atmosphere; dropwise addn. of MeOH to n-BuLi in hexane (-30°C, stirring), addn. of hexane, dropwise addn. of PhCH2GeMe2Cl (-30°C), stirring (room temp., 15 h); sepn. of LiCl (filtration), removal of solvent (20 mbar), distn.; elem. anal.;
DOI:10.1016/0022-328X(93)80293-K