(2-cyclohexyloxy-N-cyclohexylaniline)AlMe₃

Base Information

Chemical Name:(2-cyclohexyloxy-N-cyclohexylaniline)AlMe₃
CAS No.:627098-53-7
Molecular Formula:C₂₁H₃₆AlNO
Molecular Weight:345.504
Hs Code.:

(2-cyclohexyloxy-N-cyclohexylaniline)AlMe<sub>3</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-cyclohexyloxy-N-cyclohexylaniline)AlMe₃

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Technology Process of (2-cyclohexyloxy-N-cyclohexylaniline)AlMe₃

There total 1 articles about (2-cyclohexyloxy-N-cyclohexylaniline)AlMe₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-24-1
trimethylaluminum

: 627098-50-4
2-cyclohexyloxy-N-cyclohexylaniline

: 627098-53-7
(2-cyclohexyloxy-N-cyclohexylaniline)AlMe₃

Guidance literature:: In pentane; under N2; ligand dissolved in pentane; stored at -35°C for 30 min; taken out of freezer; AlMe3 (1 equiv.) added quickly; warmed to room temp.; stirred at room temp. for 1 h; stored at -35°C overnight; filtered through glass frit; dried under vac.; detd. by (1)H NMR spectra; Al adduct contained minor impurities;
DOI:10.1016/S0022-328X(03)00790-3

Reference yield:

: 627098-53-7
(2-cyclohexyloxy-N-cyclohexylaniline)AlMe₃

: 627098-54-8
(2-cyclohexyloxy-N-(cyclohexyl)phenylamido)AlMe₂

Guidance literature:: In benzene-d6; byproducts: CH4; under N2; Al complex in C6D6 decompd. at 75°C for 18 h; detd. by (1)H NMR spectra;
DOI:10.1016/S0022-328X(03)00790-3