Ethenesulfonic acid, 4-methoxyphenyl ester

Base Information

• Chemical Name: Ethenesulfonic acid, 4-methoxyphenyl ester
• CAS No.: 3441-82-5
• Molecular Formula: C9H10O4S
• Molecular Weight: 214.242

Synonyms:

Chemical Property of Ethenesulfonic acid, 4-methoxyphenyl ester

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of Ethenesulfonic acid, 4-methoxyphenyl ester

There total 1 articles about Ethenesulfonic acid, 4-methoxyphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2-Chloroethanesulfonyl chloride (1622-32-8) + 4-methoxy-phenol (150-76-5) → ethenesulfonic acid 4-methoxyphenyl ester (3441-82-5)

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃; for 12h; Inert atmosphere;

DOI:10.1021/acs.jmedchem.5b00099

Reference yield: 92.0%

ethenesulfonic acid 4-methoxyphenyl ester (3441-82-5) + 8-((4-(4-(4-hydroxyphenyl)furan-3-yl)phenyl)amino)-8-oxooctanoic acid → 8-(4-(3-(4-hydroxyphenyl)-6-(4-methoxyphenoxysulfonyl)-7-oxabicyclo[2.2.1]hept-2-en-2-yl)phenylamino)-8-oxooctanoic acid

Guidance literature:

In neat (no solvent); at 90 ℃; for 12h; Inert atmosphere;

DOI:10.1021/acs.jmedchem.5b00099

Reference yield: 75.0%

ethenesulfonic acid 4-methoxyphenyl ester (3441-82-5) → ethenesulfonic acid 4-hydroxyphenyl ester (870614-41-8)

Guidance literature:

With boron dimethyl-trifluoro sulphide; In dichloromethane; at 20 ℃; for 18h;

DOI:10.1021/jm0506773

upstream raw materials:

2-Chloroethanesulfonyl chloride

4-methoxy-phenol

Downstream raw materials:

ethenesulfonic acid 4-hydroxyphenyl ester

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