2-Methyl-3-(2-methylphenyl)thiophene

Base Information

Chemical Name:2-Methyl-3-(2-methylphenyl)thiophene
CAS No.:345306-46-9
Molecular Formula:C12H12S
Molecular Weight:188.293
Hs Code.:
DSSTox Substance ID:DTXSID601291450

Synonyms:2-methyl-3-(2-methylphenyl)thiophene;SCHEMBL22023520;DTXSID601291450;345306-46-9

Suppliers and Price of 2-Methyl-3-(2-methylphenyl)thiophene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Methyl-3-(2-methylphenyl)thiophene

Chemical Property:

XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:188.06597156
Heavy Atom Count:13
Complexity:167

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=CC=C1C2=C(SC=C2)C

Technology Process of 2-Methyl-3-(2-methylphenyl)thiophene

There total 1 articles about 2-Methyl-3-(2-methylphenyl)thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 30319-05-2
3-bromo-2-methylthiophene

: 932-31-0
ortho-tolylmagnesium bromide

: 345306-46-9
2-methyl-3-(2-methylphenyl)thiophene

Guidance literature:: With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); In diethyl ether;
DOI:10.1021/ja004266h

Reference yield:

: 79-41-4,25087-26-7,50867-57-7
poly(methacrylic acid)

: 345306-46-9
2-methyl-3-(2-methylphenyl)thiophene

: 345306-47-0
2,5-dimethyl-3-(2-methylphenyl)-5,6-dihydrocyclopenta[1,2-b]thiophen-4-one

Guidance literature:: With PPA; In 1,2-dichloro-ethane; at 80 ℃; for 5h;
DOI:10.1021/ja004266h

Reference yield:

: 345306-46-9
2-methyl-3-(2-methylphenyl)thiophene

: 2,5-dimethyl-3-(2-methylphenyl)-5-hydrocyclopenta[1,2-b]thiophene

Guidance literature:: Multi-step reaction with 2 steps

1.1: PPA / 1,2-dichloro-ethane / 5 h / 80 °C

2.1: LiAlH₄ / tetrahydrofuran / 3 h / 20 °C

2.2: p-TSA / toluene / 1.5 h / 70 °C

With lithium aluminium tetrahydride; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1021/ja004266h