cyclohexene-1-¹³C

Base Information

• Chemical Name: cyclohexene-1-¹³C
• CAS No.: 1192-09-2
• Molecular Formula: C₆H₁₀
• Molecular Weight: 83.1344
• Mol file: 1192-09-2.mol

Synonyms:

Chemical Property of cyclohexene-1-¹³C

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cyclohexene-1-¹³C

There total 2 articles about cyclohexene-1-¹³C which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexanol-1-13C (38134-57-5) → cyclohexene-3-13C + cyclohexene-4-13C + cyclohexene-1-13C (1192-09-2) + <2-(13)C>-cyclohexanol (133499-74-8) + <3-(13C)>-cyclohexanol (133499-75-9) + <4-(13C)>-cyclohexanol (133499-76-0)

Guidance literature:

With zeolite HBEA₁₅₀; In water; at 130 ℃; for 22.4h; Concentration; Catalytic behavior; Kinetics; Autoclave;

DOI:10.1002/anie.201306673

Reference yield:

→ cyclohexene-1-13C (1192-09-2)

Guidance literature:

Ethyl-<1-C¹³>cyclohexyl-carbonat, 450grad;

DOI:10.1021/jo01034a055

upstream raw materials:

cyclohexanol-1-13C

Refernces

• 1、 Vjunov, Aleksei,Hu, Mary Y.,Feng, Ju,Camaioni, Donald M.,Mei, Donghai,Hu, Jian Z.,Zhao, Chen,Lercher, Johannes A.. "Following solid-acid-catalyzed reactions by MAS NMR spectroscopy in liquid phase - Zeolite-catalyzed conversion of cyclohexanol in water". supporting information. p. 479 - 482. Retrieved 2014/01/23.