1-Dibenzothiophenemethanol

Base Information

• Chemical Name: 1-Dibenzothiophenemethanol
• CAS No.: 34724-70-4
• Molecular Formula: C13H10OS
• Molecular Weight: 214.288
• Mol file: 34724-70-4.mol

Synonyms:

Chemical Property of 1-Dibenzothiophenemethanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Dibenzothiophenemethanol

There total 6 articles about 1-Dibenzothiophenemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

dibenzo[b,d]thiophene-1-carbaldehyde (91538-74-8) → dibenzo[b,d]thiophen-1-ylmethanol (34724-70-4)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.5h; Inert atmosphere;

DOI:10.1002/anie.201100775

Reference yield: 90.0%

dibenzothiophene-1-carboxylic acid (34724-68-0) → dibenzo[b,d]thiophen-1-ylmethanol (34724-70-4)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 3h; Heating;

Reference yield:

ethyl dibenzothiophene-1-carboxylate (34724-71-5) → dibenzo[b,d]thiophen-1-ylmethanol (34724-70-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 94 percent / 10percent NaOH / methanol / 2.5 h / Heating

2: 90 percent / LiAlH₄ / diethyl ether / 3 h / Heating

With sodium hydroxide; lithium aluminium tetrahydride; In methanol; diethyl ether;

upstream raw materials:

dibenzothiophene-1-carboxylic acid

ethyl dibenzothiophene-1-carboxylate

dibenzo[b,d]thiophene-1-carbaldehyde

benzyl phenyl sulfoxide

Downstream raw materials:

1-methyldibenzo[b,d]thiophene

2-methylbiphenyl