Butyl 3-(2-hydroxyphenyl)prop-2-enoate

Base Information

Chemical Name:Butyl 3-(2-hydroxyphenyl)prop-2-enoate
CAS No.:3487-90-9
Molecular Formula:C13H16O3
Molecular Weight:220.268
Hs Code.:
DSSTox Substance ID:DTXSID50706969
Mol file:3487-90-9.mol

Synonyms:Butyl 3-(2-hydroxyphenyl)prop-2-enoate;3487-90-9;DTXSID50706969

Suppliers and Price of Butyl 3-(2-hydroxyphenyl)prop-2-enoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Butyl 3-(2-hydroxyphenyl)prop-2-enoate

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:220.109944368
Heavy Atom Count:16
Complexity:235

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCOC(=O)C=CC1=CC=CC=C1O

Technology Process of Butyl 3-(2-hydroxyphenyl)prop-2-enoate

There total 7 articles about Butyl 3-(2-hydroxyphenyl)prop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 141-32-2,9003-49-0
acrylic acid n-butyl ester

: 533-58-4
2-Iodophenol

: 3487-90-9
n-butyl (E)-3-(o-hydroxyphenyl)acrylate

Guidance literature:: With triethylamine; bis(N-methylimidazol-2-yl)Pd(Cl)Me; In various solvent(s); at 120 ℃; for 1h;
DOI:10.1021/ol030071d

Reference yield: 84.0%

: 141-32-2,9003-49-0
acrylic acid n-butyl ester

: 90-02-8
salicylaldehyde

: 3487-90-9
n-butyl (E)-3-(o-hydroxyphenyl)acrylate

Guidance literature:: With dicarbonylacetylacetonato rhodium (I); In N,N-dimethyl-formamide; at 120 ℃; for 3h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.joc.9b00602

Reference yield:

: 141-32-2,9003-49-0
acrylic acid n-butyl ester

: 95-56-7
2-hydroxybromobenzene

: 3487-90-9
n-butyl (E)-3-(o-hydroxyphenyl)acrylate

Guidance literature:: With potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); (1RS,2RS,3SR,4SR)-1,2,3,4-tetrakis((diphenylphosphanyl)methyl)cyclopentane; In N,N-dimethyl-formamide; at 130 ℃; for 20h;
DOI:10.1055/s-2001-18752